RESUMEN
Present study was conducted to develop a stable chia oil emulsion using an ultrasound emulsification technique. Whey protein concentrate, gum Arabic, and xanthan gum stabilized layer by layer chia oil emulsion was developed using an electrostatic deposition. Single-layer and multilayer emulsion of chia oil was developed and their stability is compared. Developed emulsions were characterized by viscosity, stability, surface charge, and droplet size. Layer-by-layer emulsion showed the highest stability (98%) among all the formulations developed. Formulated single-layer and double-layer emulsions were spray dried and the respective powders were characterized for bulk density, tapped density, Hausner ratio, Carr's index, moisture content, color values, encapsulation efficiency, peroxide value, XRD, and SEM. Multilayer emulsion-based powder showed better flowability properties. The encapsulation efficiency of multilayer microparticles was found to be 93% with the lowest peroxide value of 1.08 mEq O2/kg fat. XRD diffractogram of the developed microparticles revealed amorphous nature. The developed ultrasound layer-by-layer emulsification technique is an efficient technique for developing chia oil-loaded microparticles.
RESUMEN
Current research aims to evaluate the effect of high shear extrusion on quinoa, finger millet, and red rice composite flour-based breakfast cereal using response surface methodology with extruder barrel temperature (120-130 °C), screw speed (320-350 rpm) and feed moisture content (10-20 g/100 g) as independent variables. Product responses were fitted on to mathematical model using second-order polynomial equations. Multiple regression analysis of data revealed the high statistical significance of respective mathematical models. Numeric optimization based on acceptable product characteristics revealed optimized processing conditions (barrel temperature 130 °C, screw speed 350 RPM, and feed moisture content 20 g/100 g) with a desirability of 0.9373. Extrudates developed using selected processing conditions along with optimized ones and control were characterized for their nutrient profile and crystallinity. Breakfast cereal developed using optimized processing conditions showed a better nutritional profile and reduction in crystallinity of product after high shear extrusion processing represented starch gelatinization.