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Miniaturized sample preparation techniques and ambient mass spectrometry as approaches for food residue analysis.
Martins, Rafael Oliveira; de Araújo, Giovanna Lopes; de Freitas, Carla Santos; Silva, Allyster Rodrigues; Simas, Rosineide Costa; Vaz, Boniek Gontijo; Chaves, Andrea Rodrigues.
Afiliação
  • Martins RO; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
  • de Araújo GL; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
  • de Freitas CS; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
  • Silva AR; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
  • Simas RC; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
  • Vaz BG; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
  • Chaves AR; Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.
J Chromatogr A ; 1640: 461949, 2021 Mar 15.
Article em En | MEDLINE | ID: mdl-33556677
Analytical methods such as liquid chromatography (LC) and mass spectrometry (MS) are widely used techniques for the analyses of different classes of compounds. This is due to their highlighted capacity for separating and identifying components in complex matrices such food samples. However, in most cases, effective analysis of the target analyte becomes challenging due to the complexity of the sample, especially for quantification of trace concentrations. In this case, miniaturized sample preparation methods have been used as a strategy for analysis of complex matrices. This involves removing the interferents and concentrating the analytes in a sample. These methods combine simplicity and effectiveness and given their miniaturized scale, they are in accordance with green chemistry precepts. Besides, ambient mass spectrometry represents a new trend in fast and rapid analyses, especially for qualitative and screening analysis. However, for complex matrix analyses, sample preparation is still a difficult step and the miniaturized sample preparation techniques show great potential for an improved and widespread use of ambient mass spectrometry techniques. . This review aims to contribute as an overview of current miniaturized sample preparation techniques and ambient mass spectrometry methods as different approaches for selective and sensitive analysis of residues in food samples.
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Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Espectrometria de Massas / Análise de Alimentos / Miniaturização Tipo de estudo: Qualitative_research Idioma: En Revista: J Chromatogr A Ano de publicação: 2021 Tipo de documento: Article País de afiliação: Brasil País de publicação: Holanda

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Espectrometria de Massas / Análise de Alimentos / Miniaturização Tipo de estudo: Qualitative_research Idioma: En Revista: J Chromatogr A Ano de publicação: 2021 Tipo de documento: Article País de afiliação: Brasil País de publicação: Holanda