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Chemical and Mechanical Properties of Experimental Dental Composites as a Function of Formulation and Postcuring Thermal Treatment.
Esteves, Renata A; Boaro, Letícia C C; Gonçalves, Flávia; Campos, Luiza M P; Silva, Cecy M; Rodrigues-Filho, Leonardo Eloy.
Afiliação
  • Esteves RA; School of Dentistry, University Federal of Pará, Rua Augusto Corrêa 01, 66075-110 Belém, PA, Brazil.
  • Boaro LCC; School of Dentistry, University of Santo Amaro, Rua Professor Enéas de Siqueira Neto 340, 04829-300 São Paulo, SP, Brazil.
  • Gonçalves F; University Ibirapuera, Av. Interlagos 1329, 04661-100 São Paulo, SP, Brazil.
  • Campos LMP; Nuclear and Energy Research Institute, University of São Paulo, Av. Lineu Prestes 2242, 05508-000 São Paulo, SP, Brazil.
  • Silva CM; School of Dentistry, University Federal of Pará, Rua Augusto Corrêa 01, 66075-110 Belém, PA, Brazil.
  • Rodrigues-Filho LE; Department of Biomaterials and Oral Biology, School of Dentistry, University of São Paulo, Av. Lineu Prestes 2227, 05508-900 São Paulo, SP, Brazil.
Biomed Res Int ; 2018: 9845427, 2018.
Article em En | MEDLINE | ID: mdl-29736401
This study evaluated the influence of formulation and thermal treatment on the degree of conversion, fracture toughness, flexural strength, and elastic modulus of experimental composites. Six composites were analyzed at BisGMA : TEGDMA molar ratios of 1 : 1 and 7 : 3 with filler at 30, 50, and 70 wt%. The degree of conversion was analyzed by Fourier transform infrared spectroscopy, fracture toughness was measured using the single-edge notched beam, and flexural strength and elastic modulus were measured with the 3-point bend test. For all tests, one-half of the specimens received thermal treatment at 170°C for 10 min. Data were analyzed by the Kruskal-Wallis or ANOVA/Tukey's test (α = 5%). The 1 : 1 BisGMA : TEGDMA ratio showed higher properties than the 7 : 3 ratio. Although the material with 70% filler had a conversion lower than the one with 50%, it showed higher mechanical properties. The thermal treatment improved all properties in all materials. Therefore, the use of an equimolar ratio of BisGMA : TEGDMA can be paired with 70 wt% filler to design dental composites that possess increased advantageous physical and chemical properties. Furthermore, the simple and low-cost method of thermal treatment proposed for use in clinical dentistry has been shown to effectively improve the properties of all evaluated materials.
Assuntos

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Estresse Mecânico / Bis-Fenol A-Glicidil Metacrilato / Resinas Compostas Limite: Humans Idioma: En Revista: Biomed Res Int Ano de publicação: 2018 Tipo de documento: Article País de afiliação: Brasil País de publicação: Estados Unidos

Texto completo: 1 Coleções: 01-internacional Base de dados: MEDLINE Assunto principal: Estresse Mecânico / Bis-Fenol A-Glicidil Metacrilato / Resinas Compostas Limite: Humans Idioma: En Revista: Biomed Res Int Ano de publicação: 2018 Tipo de documento: Article País de afiliação: Brasil País de publicação: Estados Unidos