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A simple method of preparation for [123I]-(S)-(-)-IBZM.
Wang, T S; Malaspina, D; Van Heertum, R L.
Afiliación
  • Wang TS; Department of Radiology, College of Physicians and Surgeons, Columbia University, New York, NY 10032, USA.
Appl Radiat Isot ; 49(4): 369-72, 1998 Apr.
Article en En | MEDLINE | ID: mdl-9519443
Sterile, apyrogenic [123I]IBZM was prepared in a sealed, capped 'V' vial, followed by SEP-PAK C-18 cartridge purification, and then was placed under sealed vial condensation. The quantity of BZM present in the final product ranged from 3.3-5.9 micrograms, as measured by a UV spectrophotometer at 254 and 308 nm. Animal biodistribution studies revealed that the [123I]IBZM prepared by this method which contained 5.9 micrograms of BZM, compared to the standard preparation method containing 0 microgram of BZM, resulted in identical brain uptakes at 15, 30, 60, and 120 min post-injection. The in vitro and in vivo studies demonstrated that a small amount of BZM presence in the final product did not affect the radiochemical purity, nor the D2 receptor binding capacity in the rat brain of [123I]IBZM. The preparation time can be shortened to 1.5 h compared with at least 2-4 h needed for the standard method of preparation. This factor may be important in routine clinical application.
Asunto(s)
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Pirrolidinas / Benzamidas / Antagonistas de Dopamina / Medios de Contraste / Radioisótopos de Yodo Límite: Animals Idioma: En Revista: Appl Radiat Isot Asunto de la revista: MEDICINA NUCLEAR / SAUDE AMBIENTAL Año: 1998 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Reino Unido
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Pirrolidinas / Benzamidas / Antagonistas de Dopamina / Medios de Contraste / Radioisótopos de Yodo Límite: Animals Idioma: En Revista: Appl Radiat Isot Asunto de la revista: MEDICINA NUCLEAR / SAUDE AMBIENTAL Año: 1998 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Reino Unido