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A capillary gas-liquid chromatographic method for the assay of the neuroleptic drug zotepine in human serum or plasma.
Ulrich, S; Meyer, F P; Bogerts, B.
Afiliación
  • Ulrich S; Institute of Clinical Pharmacology, University Hospital, Magdeburg, Germany.
J Pharm Biomed Anal ; 14(4): 441-9, 1996 Feb.
Article en En | MEDLINE | ID: mdl-8729643
A capillary gas-liquid chromatographic method suitable for the assay of the atypical neuroleptic drug zotepine in human serum or plasma was developed. A liquid-liquid extraction with three subsequent extraction steps was applied for sample preparation. The minimum detectable concentration was 1.0 ng ml-1. The within-day relative standard deviation (RSD) (n = 6) was 5.3% at 5 ng ml-1, 3.6% at 10 ng ml-1 and 6.1% at 100 ng ml-1. The day-to-day RSD (n = 6) was 9.3% at 10 ng ml-1 and 5.1% at 100 ng ml-1. Steady-state serum levels of four schizophrenic patients were measured.
Asunto(s)
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Antipsicóticos / Dibenzotiepinas Límite: Adult / Female / Humans / Male Idioma: En Revista: J Pharm Biomed Anal Año: 1996 Tipo del documento: Article País de afiliación: Alemania Pais de publicación: Reino Unido
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Antipsicóticos / Dibenzotiepinas Límite: Adult / Female / Humans / Male Idioma: En Revista: J Pharm Biomed Anal Año: 1996 Tipo del documento: Article País de afiliación: Alemania Pais de publicación: Reino Unido