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Reaction-Free Energies for Complexation of Carbohydrates by Tweezer Diboronic Acids.
Lara-Cruz, Gustavo Adolfo; Rose, Thomas; Grimme, Stefan; Jaramillo-Botero, Andres.
Afiliación
  • Lara-Cruz GA; iOMICAS Research Institute, Pontificia Universidad Javeriana, Calle 17 # 121B-155, Santiago de Cali, Valle del Cauca 760031, Colombia.
  • Rose T; Mulliken Center for Theoretical Chemistry, Clausius-Institut für Physikalische und Theoretische Chemie, Rheinische Friedrich-Wilhelms Universität Bonn, Beringstraße 4, Bonn 53115, Germany.
  • Grimme S; Mulliken Center for Theoretical Chemistry, Clausius-Institut für Physikalische und Theoretische Chemie, Rheinische Friedrich-Wilhelms Universität Bonn, Beringstraße 4, Bonn 53115, Germany.
  • Jaramillo-Botero A; iOMICAS Research Institute, Pontificia Universidad Javeriana, Calle 17 # 121B-155, Santiago de Cali, Valle del Cauca 760031, Colombia.
J Phys Chem B ; 128(38): 9213-9223, 2024 Sep 26.
Article en En | MEDLINE | ID: mdl-39284008
ABSTRACT
The accurate calculation of reaction-free energies (ΔrG°) for diboronic acids and carbohydrates is challenging due to reactant flexibility and strong solute-solvent interactions. In this study, these challenges are addressed with a semiautomatic workflow based on quantum chemistry methods to calculate conformational free energies, generate microsolvated solute structural ensembles, and compute ΔrG°. Workflow parameters were optimized for accuracy and precision while controlling computational costs. We assessed the accuracy by studying three reactions of diboronic acids with glucose and galactose, finding that the conformational entropy contributes significantly (by 3-5 kcal/mol at room temperature). Explicit solvent molecules improve the computed ΔrG° accuracy by about 4 kcal/mol compared to experimental data, though using 13 or more water molecules reduced precision and increased computational overhead. After fine-tuning, the workflow demonstrated remarkable accuracy, with an absolute error of about 2 kcal/mol compared to experimental ΔrG° and an average interquartile range of 2.4 kcal/mol. These results highlight the workflow's potential for designing and screening tweezer-like ligands with tailored selectivity for various carbohydrates.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: J Phys Chem B Asunto de la revista: QUIMICA Año: 2024 Tipo del documento: Article País de afiliación: Colombia Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: J Phys Chem B Asunto de la revista: QUIMICA Año: 2024 Tipo del documento: Article País de afiliación: Colombia Pais de publicación: Estados Unidos