Your browser doesn't support javascript.
loading
Evaluation of polypropylene CSF low-bind collection tubes for trace metal contamination.
Bitzer, Anna C; Jannetto, Paul J; Bornhorst, Joshua A.
Afiliación
  • Bitzer AC; Department of Laboratory Medicine and Pathology, Mayo Clinic, Rochester, MN, US.
  • Jannetto PJ; Department of Laboratory Medicine and Pathology, Mayo Clinic, Rochester, MN, US.
  • Bornhorst JA; Department of Laboratory Medicine and Pathology, Mayo Clinic, Rochester, MN, US.
Lab Med ; 2024 Aug 13.
Article en En | MEDLINE | ID: mdl-39136221
ABSTRACT

BACKGROUND:

Due to the ability of metal ions to cross the blood-brain barrier, there has been interest in analyzing cerebrospinal fluid (CSF) for trace element concentrations to investigate possible correlations with neurodegenerative diseases. In this study, Sarstedt polypropylene CSF collection tubes were analyzed to determine the contamination levels of aluminum, titanium, chromium, manganese, cobalt, nickel, molybdenum, gadolinium, vanadium, arsenic, cadmium, mercury, lead, thallium, selenium, copper, zinc, and iron.

METHODS:

Sarstedt polypropylene CSF collection tubes from 2 separate lots (n = 10 per lot) were filled with a 2 mL aliquot of a CSF pool with known element concentrations. After 24 hours of leaching at room temperature, all 18 elements were analyzed via inductively coupled plasma mass spectrometry (ICP-MS). Results were subtracted from the initial pool concentration to determine contamination levels.

RESULTS:

No detectable contamination above the assay limit of detection was found in 11 analytes. Molybdenum and selenium contamination was measured in all tubes, and aluminum, titanium, manganese, thallium, and zinc had minimal levels of sporadic detectable contamination in 25% or fewer of the tubes tested.

CONCLUSIONS:

Sarstedt polypropylene CSF tubes are an acceptable collection tube for the analysis of most assessed metals in CSF.
Palabras clave

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Lab Med Año: 2024 Tipo del documento: Article Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Lab Med Año: 2024 Tipo del documento: Article Pais de publicación: Reino Unido