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Analysis of Carbon Materials with Infrared Photoacoustic Spectroscopy.
Tseng, Ton-Rong; Yang, Che-Hua; Lu, Hsiao-Chi; Liu, Ching-Ping; Cheng, Bing-Ming.
Afiliación
  • Tseng TR; College of Mechanical and Electrical Engineering, National Taipei University of Technology, 1, Sec. 3, Zhongxiao E. Rd., Taipei 10608, Taiwan.
  • Yang CH; College of Mechanical and Electrical Engineering, National Taipei University of Technology, 1, Sec. 3, Zhongxiao E. Rd., Taipei 10608, Taiwan.
  • Lu HC; Department of Medical Research, Hualien Tzu Chi Hospital, Buddhist Tzu Chi Medical Foundation, No. 707, Sec. 3, Chung-Yang Rd., Hualien City 970, Taiwan.
  • Liu CP; Department of Chemistry, Fu Jen Catholic University, 510 Zhongzheng Rd., Xinzhuang, New Taipei City 242062, Taiwan.
  • Cheng BM; Department of Medical Research, Hualien Tzu Chi Hospital, Buddhist Tzu Chi Medical Foundation, No. 707, Sec. 3, Chung-Yang Rd., Hualien City 970, Taiwan.
Anal Chem ; 96(26): 10732-10737, 2024 Jul 02.
Article en En | MEDLINE | ID: mdl-38875498
ABSTRACT
Measurement of infrared spectroscopy has emerged as a significant challenge for carbon materials due to the sampling problem. To overcome this issue, in this work, we performed measurements of IR spectra for carbon materials including C60, C70, diamond powders, graphene, and carbon nanotubes (CNTs) using the photoacoustic spectroscopy (PAS) technique; for comparison, the vibrational patterns of these materials were also studied with a conventional transmission method, diffuse reflectance infrared Fourier transform (DRIFT) spectroscopy, or Raman spectroscopy. We found that the IR photoacoustic spectroscopy (IR-PAS) scheme worked successfully for these carbon materials, offering advantages in sampling. Interestingly, the profiles of IR-PAS spectra for graphene and CNTs exhibit negative bands using carbon black as the reference; the negative spectral information may provide valuable knowledge about the storage energy, production, structure, defect, or impurity of graphene and CNTs. Thus, this approach may open a new avenue for analyzing carbon materials.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Anal Chem Año: 2024 Tipo del documento: Article País de afiliación: Taiwán Pais de publicación: Estados Unidos
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
Buscar en Google

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Anal Chem Año: 2024 Tipo del documento: Article País de afiliación: Taiwán Pais de publicación: Estados Unidos