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The two-step strategy for enhancing the specific activity and thermostability of alginate lyase AlyG2 with mechanism for improved thermostability.
Huang, Jin-Ping; Yun, Shuai-Ting; Zhao, Jin-Xin; Wang, Xue-Ting; Wang, Xiao-Chen; Guo, Xiang-Yi; San, Dong-Mei; Zhou, Yan-Xia.
Afiliación
  • Huang JP; Marine College, Shandong University, Weihai, Shandong 264209, China.
  • Yun ST; Marine College, Shandong University, Weihai, Shandong 264209, China.
  • Zhao JX; Monash Biomedicine Discovery Institute, Infection Program and Department of Microbiology, Monash University, Clayton, Victoria 3800, Australia.
  • Wang XT; Marine College, Shandong University, Weihai, Shandong 264209, China.
  • Wang XC; Marine College, Shandong University, Weihai, Shandong 264209, China.
  • Guo XY; SDU-ANU joint science college, Shandong University, Weihai, Shandong 264209, China.
  • San DM; Marine College, Shandong University, Weihai, Shandong 264209, China.
  • Zhou YX; Marine College, Shandong University, Weihai, Shandong 264209, China.
Int J Biol Macromol ; 273(Pt 2): 132685, 2024 Jul.
Article en En | MEDLINE | ID: mdl-38823749
ABSTRACT
To overcome the trade-off challenge encountered in the engineering of alginate lyase AlyG2 from Seonamhaeicola algicola Gy8T and to expand its potential industrial applications, we devised a two-step strategy encompassing activity enhancement followed by thermal stability engineering. To enhance the specific activity of efficient AlyG2, we strategically substituted residues with bulky steric hindrance proximal to the active pocket with glycine or alanine. This led to the generation of three promising positive mutants, with particular emphasis on the T91S mutant, exhibiting a 1.91-fold specific activity compared to the wild type. To mitigate the poor thermal stability of T91S, mutants with negative ΔΔG values in the thermal flexibility region were screened out. Notably, the S72Ya mutant not only displayed 17.96 % further increase in specific activity but also exhibited improved stability compared to T91S, manifesting as a remarkable 30.97 % increase in relative activity following a 1-hour incubation at 42 °C. Furthermore, enhanced kinetic stability was observed. To gain deeper insights into the mechanism underlying the enhanced thermostability of the S72Ya mutant, we conducted molecular dynamics simulations, principal component analysis (PCA), dynamic cross-correlation map (DCCM), and free energy landscape (FEL) analysis. The results unveiled a reduction in the flexibility of the surface loop, a stronger correlation dynamic and a narrower motion subspace in S72Ya system, along with the formation of more stable hydrogen bonds. Collectively, our findings suggest amino acids substitutions resulting in smaller side chains proximate to the active site can positively impact enzyme activity, while reducing the flexibility of surface loops emerges as a pivotal factor in conferring thermal stability. These insights offer valuable guidance and a framework for the engineering of other enzyme types.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Polisacárido Liasas / Estabilidad de Enzimas / Simulación de Dinámica Molecular Idioma: En Revista: Int J Biol Macromol Año: 2024 Tipo del documento: Article País de afiliación: China Pais de publicación: Países Bajos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Polisacárido Liasas / Estabilidad de Enzimas / Simulación de Dinámica Molecular Idioma: En Revista: Int J Biol Macromol Año: 2024 Tipo del documento: Article País de afiliación: China Pais de publicación: Países Bajos