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Enhanced N2 Adsorption and Activation by Combining Re Clusters and In Vacancies as Dual Sites for Efficient and Selective Electrochemical NH3 Synthesis.
Li, Shaoquan; Liu, Yi-Tao; Zhang, Yong-Chao; Du, Yue; Gao, Jian; Zhai, Jingru; Liang, Yue; Han, Caidi; Zhu, Xiao-Dong.
Afiliación
  • Li S; State key Laboratory Based of Eco-chemical Engineering College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao 266042, China.
  • Liu YT; School of Materials Science and Engineering, Guangdong University of Petrochemical Technology, Maoming 525000, China.
  • Zhang YC; Innovation Center for Textile Science and Technology, Donghua University, Shanghai 200051, China.
  • Du Y; State key Laboratory Based of Eco-chemical Engineering College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao 266042, China.
  • Gao J; State key Laboratory Based of Eco-chemical Engineering College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao 266042, China.
  • Zhai J; State key Laboratory Based of Eco-chemical Engineering College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao 266042, China.
  • Liang Y; Weichai Holding Group Co., Ltd., Weifang 261000, China.
  • Han C; State key Laboratory Based of Eco-chemical Engineering College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao 266042, China.
  • Zhu XD; State key Laboratory Based of Eco-chemical Engineering College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao 266042, China.
Nano Lett ; 24(2): 748-756, 2024 Jan 17.
Article en En | MEDLINE | ID: mdl-38166417
ABSTRACT
The electrochemical N2 reduction reaction (NRR) is a green and energy-saving sustainable technology for NH3 production. However, high activity and high selectivity can hardly be achieved in the same catalyst, which severely restricts the development of the electrochemical NRR. In2Se3 with partially occupied p-orbitals can suppress the H2 evolution reaction (HER), which shows excellent selectivity in the electrochemical NRR. The presence of VIn can simultaneously provide active sites and confine Re clusters through strong charge transfer. Additionally, well-isolated Re clusters stabilized on In2Se3 by the confinement effect of VIn result in Re-VIn active sites with maximum availability. By combining Re clusters and VIn as dual sites for spontaneous N2 adsorption and activation, the electrochemical NRR performance is enhanced significantly. As a result, the Re-In2Se3-VIn/CC catalyst delivers a high NH3 yield rate (26.63 µg h-1 cm-2) and high FEs (30.8%) at -0.5 V vs RHE.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Nano Lett Año: 2024 Tipo del documento: Article País de afiliación: China Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Nano Lett Año: 2024 Tipo del documento: Article País de afiliación: China Pais de publicación: Estados Unidos