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Application of Zr-MOFs based copper complex in synthesis of pyrazolo[3, 4-b]pyridine-5-carbonitriles via anomeric-based oxidation.
Tavakoli, Elham; Sepehrmansourie, Hassan; Zarei, Mahmoud; Zolfigol, Mohammad Ali; Khazaei, Ardeshir; As'Habi, Mohammad Ali.
Afiliación
  • Tavakoli E; Department of Organic Chemistry, Faculty of Chemistry, Bu-Ali-Sina University, Hamedan, 6517838965, Iran.
  • Sepehrmansourie H; Department of Organic Chemistry, Faculty of Chemistry, Bu-Ali-Sina University, Hamedan, 6517838965, Iran.
  • Zarei M; Department of Chemistry, Faculty of Science, University of Qom, Qom, 37185-359, Iran. mahmoud8103@yahoo.com.
  • Zolfigol MA; Department of Organic Chemistry, Faculty of Chemistry, Bu-Ali-Sina University, Hamedan, 6517838965, Iran. mzolfigol@yahoo.com.
  • Khazaei A; Department of Organic Chemistry, Faculty of Chemistry, Bu-Ali-Sina University, Hamedan, 6517838965, Iran. Khazaei_1326@yahoo.com.
  • As'Habi MA; Department of Phytochemistry, Medicinal Plant and Drugs Research Institute, Shahid Beheshti University, Evin, Tehran, 1983963113, Iran.
Sci Rep ; 13(1): 9388, 2023 Jun 09.
Article en En | MEDLINE | ID: mdl-37296128
In this research article, Zr-MOFs based copper complex as a novel heterogeneous and porous catalyst was designed and prepared. The structure of catalyst has verified by various techniques such as FT-IR, XRD, SEM, N2 adsorption-desorption isotherms (BET), EDS, SEM-elemental mapping, TG and DTG analysis. UiO-66-NH2/TCT/2-amino-Py@Cu(OAc)2 was used as an efficient catalyst in the synthesis of pyrazolo[3,4-b]pyridine-5-carbonitrile derivatives. The aromatization of titled molecules is performed via a cooperative vinylogous anomeric-based oxidation both under air and inert atmospheres. The unique properties of the presented method are short reaction time, high yield, reusability of catalyst, synthesis of desired product under mild and green condition.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Piridinas / Cobre Idioma: En Revista: Sci Rep Año: 2023 Tipo del documento: Article País de afiliación: Irán Pais de publicación: Reino Unido
Texto completo
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Imprimir
XML
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Piridinas / Cobre Idioma: En Revista: Sci Rep Año: 2023 Tipo del documento: Article País de afiliación: Irán Pais de publicación: Reino Unido