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Step-Economical Mechanosynthesis of Hybrid Azoles: Deciphering Their π-Orbital and Pharmacological Characteristics.
Sundaramoorthy, Ramachandran; Vadivelu, Murugan; Thirumoorthy, Kulandaivel; Karthikeyan, Kesavan; Praveen, Chandrasekar.
Afiliación
  • Sundaramoorthy R; Department of Chemistry, B. S. Abdur Rahman Crescent Institute of Science and Technology, Chennai, 600048, Tamil Nadu, India.
  • Vadivelu M; Department of Chemistry, B. S. Abdur Rahman Crescent Institute of Science and Technology, Chennai, 600048, Tamil Nadu, India.
  • Thirumoorthy K; Department of Chemistry, Saveetha School of Engineering, SIMATS, Chennai, 632014, Tamil Nadu, India.
  • Karthikeyan K; Department of Chemistry, B. S. Abdur Rahman Crescent Institute of Science and Technology, Chennai, 600048, Tamil Nadu, India.
  • Praveen C; Electrochemical Power Sources Division, CSIR-Central Electrochemical Research Institute, Karaikudi, 630003, Tamil Nadu, India.
ChemMedChem ; 18(13): e202300008, 2023 07 03.
Article en En | MEDLINE | ID: mdl-37055351
A hybrid pharmacophore strategy for unifying 1,2,3-triazole with 1,2,4-triazole cores to prepare mixed triazoles was accomplished by a ball-milling approach. The developed chemistry works under the catalysis of cupric oxide nanoparticles with salient features like one-jar operation, lower number of synthetic steps, catalyst recyclability, time-dependent product control, and good overall yields. π-Orbital properties based on theoretical calculations supported the suitability of these molecules for pharmacological screening. Therefore, the biological potency of the synthesized molecules was evaluated for antioxidant, anti-inflammatory, and anti-diabetic activities. By virtue of their proton-donating tendency, all compounds showed promising radical-scavenging activity with the inhibition level reaching up to 90 %. These molecular hybrids also exhibited anti-inflammatory and anti-diabetic potencies similar to those of standard compounds, owing to their electron-rich nature. Finally, α-amylase inhibitory potential was demonstrated in silico; significant regions necessary for enzyme inhibition were identified by hydrogen bonding interactions.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Azoles / Triazoles Tipo de estudio: Health_economic_evaluation / Prognostic_studies Idioma: En Revista: ChemMedChem Asunto de la revista: FARMACOLOGIA / QUIMICA Año: 2023 Tipo del documento: Article País de afiliación: India Pais de publicación: Alemania

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Azoles / Triazoles Tipo de estudio: Health_economic_evaluation / Prognostic_studies Idioma: En Revista: ChemMedChem Asunto de la revista: FARMACOLOGIA / QUIMICA Año: 2023 Tipo del documento: Article País de afiliación: India Pais de publicación: Alemania