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Effects of Addition of Tea Polyphenol Palmitate and Process Parameters on the Preparation of High-Purity EPA Ethyl Ester.
Ding, Xuyang; Liu, Fujun; Zheng, Rui; Pei, Xuechen; Wang, Ziye; Zhou, Dayong; Yin, Fawen.
Afiliación
  • Ding X; School of Food Science and Technology, Dalian Polytechnic University, Dalian 116034, China.
  • Liu F; Liao Fishing Group Limited Company, Dalian 116000, China.
  • Zheng R; School of Food Science and Technology, Dalian Polytechnic University, Dalian 116034, China.
  • Pei X; School of Food Science and Technology, Dalian Polytechnic University, Dalian 116034, China.
  • Wang Z; School of Food Science and Technology, Dalian Polytechnic University, Dalian 116034, China.
  • Zhou D; School of Food Science and Technology, Dalian Polytechnic University, Dalian 116034, China.
  • Yin F; National Engineering Research Center of Seafood, Dalian 116034, China.
Foods ; 12(5)2023 Feb 25.
Article en En | MEDLINE | ID: mdl-36900492
High-purity eicosapentaenoic acid (EPA) ethyl ester (EPA-EE) can be produced from an integrated technique consisting of saponification, ethyl esterification, urea complexation, molecular distillation and column separation. In order to improve the purity and inhibit oxidation, tea polyphenol palmitate (TPP) was added before the procedure of ethyl esterification. Furthermore, through the optimization of process parameters, 2:1 (mass ratio of urea to fish oil, g/g), 6 h (crystallization time) and 4:1 (mass ratio of ethyl alcohol to urea, g/g) were found to be the optimum conditions in the procedure of urea complexation. Distillate (fraction collection), 115 °C (distillation temperature) and one stage (the number of stages) were found to be the optimum conditions for the procedure of molecular distillation. With the addition of TPP and the above optimum conditions, high-purity (96.95%) EPA-EE was finally obtained after column separation.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Foods Año: 2023 Tipo del documento: Article País de afiliación: China Pais de publicación: Suiza

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Foods Año: 2023 Tipo del documento: Article País de afiliación: China Pais de publicación: Suiza