Your browser doesn't support javascript.
loading
Pyrazole Ureas as Low Dose, CNS Penetrant Glucosylceramide Synthase Inhibitors for the Treatment of Parkinson's Disease.
Roecker, Anthony J; Schirripa, Kathy M; Loughran, H Marie; Tong, Ling; Liang, Tao; Fillgrove, Kerry L; Kuo, Yuhsin; Bleasby, Kelly; Collier, Hannah; Altman, Michael D; Ford, Melissa C; Drolet, Robert E; Cosden, Mali; Jinn, Sarah; Hatcher, Nathan G; Yao, Lihang; Kandebo, Monika; Vardigan, Joshua D; Flick, Rosemarie B; Liu, Xiaomei; Minnick, Christina; Price, Laura A; Watt, Marla L; Lemaire, Wei; Burlein, Christine; Adam, Gregory C; Austin, Lauren A; Marcus, Jacob N; Smith, Sean M; Fraley, Mark E.
Afiliación
  • Roecker AJ; Discovery Chemistry, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Schirripa KM; Discovery Chemistry, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Loughran HM; Discovery Chemistry, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Tong L; Discovery Chemistry, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Liang T; Discovery Process Chemistry, Merck & Co., Inc., Kenilworth, New Jersey 07033, United States.
  • Fillgrove KL; ADME & Discovery Toxicology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Kuo Y; ADME & Discovery Toxicology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Bleasby K; ADME Transporters, Merck & Co., Inc., Rahway, New Jersey 07065, United States.
  • Collier H; ADME Transporters, Merck & Co., Inc., Rahway, New Jersey 07065, United States.
  • Altman MD; Computational and Structural Chemistry, Merck & Co., Inc., Boston, Massachusetts 02115, United States.
  • Ford MC; Computational and Structural Chemistry, Merck & Co., Inc., Boston, Massachusetts 02115, United States.
  • Drolet RE; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Cosden M; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Jinn S; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Hatcher NG; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Yao L; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Kandebo M; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Vardigan JD; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Flick RB; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Liu X; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Minnick C; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Price LA; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Watt ML; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Lemaire W; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Burlein C; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Adam GC; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Austin LA; Discovery Pharmaceutical Sciences, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Marcus JN; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Smith SM; Discovery Biology, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
  • Fraley ME; Discovery Chemistry, Merck & Co., Inc., West Point, Pennsylvania 19486, United States.
ACS Med Chem Lett ; 14(2): 146-155, 2023 Feb 09.
Article en En | MEDLINE | ID: mdl-36793422
Parkinson's disease is the second most prevalent progressive neurodegenerative disorder characterized by the loss of dopaminergic neurons in the substantia nigra. Loss-of-function mutations in GBA, the gene that encodes for the lysosomal enzyme glucosylcerebrosidase, are a major genetic risk factor for the development of Parkinson's disease potentially through the accumulation of glucosylceramide and glucosylsphingosine in the CNS. A therapeutic strategy to reduce glycosphingolipid accumulation in the CNS would entail inhibition of the enzyme responsible for their synthesis, glucosylceramide synthase (GCS). Herein, we report the optimization of a bicyclic pyrazole amide GCS inhibitor discovered through HTS to low dose, oral, CNS penetrant, bicyclic pyrazole urea GCSi's with in vivo activity in mouse models and ex vivo activity in iPSC neuronal models of synucleinopathy and lysosomal dysfunction. This was accomplished through the judicious use of parallel medicinal chemistry, direct-to-biology screening, physics-based rationalization of transporter profiles, pharmacophore modeling, and use a novel metric: volume ligand efficiency.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Prognostic_studies / Risk_factors_studies Idioma: En Revista: ACS Med Chem Lett Año: 2023 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Prognostic_studies / Risk_factors_studies Idioma: En Revista: ACS Med Chem Lett Año: 2023 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos