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Study of Mesalazine Solubility in Ternary Mixtures of Ethanol, Propylene Glycol, and Water at Various Temperatures.
Rahimpour, Elaheh; Martinez, Fleming; Hemmati, Salar; Ramezani, Amir M; Jouyban, Abolghasem.
Afiliación
  • Rahimpour E; Pharmaceutical Analysis Research Center and Faculty of Pharmacy, Tabriz University of Medical sciences, Tabriz, Iran; Food and Drug Safety Research Center, Tabriz University of Medical Sciences, Tabriz, Iran.
  • Martinez F; Grupo de Investigaciones Farmacéutico-Fisicoquímicas, Departamento de Farmacia, Facultad de Ciencias, Universidad Nacional de Colombia - Sede Bogotá, Cra. 30 No. 45-03, Bogotá, D.C., Colombia.
  • Hemmati S; Drug Applied Research Center, Tabriz University of Medical Sciences, Tabriz, Iran.
  • Ramezani AM; Healthy Ageing Research Centre, Neyshabur University of Medical Sciences, Neyshabur, Iran. Electronic address: ramezania@nums.ac.ir.
  • Jouyban A; Pharmaceutical Analysis Research Center and Faculty of Pharmacy, Tabriz University of Medical sciences, Tabriz, Iran; Faculty of Pharmacy, Near East University, PO BOX: 99138 Nicosia, North Cyprus, Mersin 10, Turkey.
J Pharm Sci ; 111(10): 2758-2764, 2022 10.
Article en En | MEDLINE | ID: mdl-35908653
Mesalazine is a low-permeable and low-soluble drug, which makes it a class IV drug in the Biopharmaceutics Classification System. Hence, its solubilization can be helpful for various stages of formulation development. The purpose of this study was to investigate the solubilization manner and thermodynamics of mesalazine in ternary solvent combinations of {ethanol (1) + propylene glycol (2) + water (3)} using the shake-flask technique at (298.2-313.2) K. In the following, the mathematical representation of the acquired solubility data using some popular models was evaluated. The accuracies of the applied models were described by percentages of mean relative deviation (MRD%). Based on obtained results (MRD% < 10.0), it can be concluded that the trained models can adequately predict the solubility of mesalazine in the investigated ternary solvent combinations. The findings also revealed that the solution composition and temperatures greatly influence the solubility of mesalazine. In addition, the thermodynamic characteristics of the mesalazine dissolution process indicate that the mesalazine dissolution process is endothermic and entropy-driven. The generating data in the current work also expands the available solubility database for mesalazine in the solvent mixtures.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Agua / Etanol Tipo de estudio: Prognostic_studies Idioma: En Revista: J Pharm Sci Año: 2022 Tipo del documento: Article País de afiliación: Irán Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Agua / Etanol Tipo de estudio: Prognostic_studies Idioma: En Revista: J Pharm Sci Año: 2022 Tipo del documento: Article País de afiliación: Irán Pais de publicación: Estados Unidos