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Chiral ionic liquids supported on natural sporopollenin microcapsules.
Palazzo, Ivan; Mezzetta, Andrea; Guazzelli, Lorenzo; Sartini, Stefania; Pomelli, Christian Silvio; Parker, Wallace O; Chiappe, Cinzia.
Afiliación
  • Palazzo I; Dipartimento di Farmacia, Università di Pisa Via Bonanno 33 56126 Pisa Italy cinzia.chiappe@unipi.it lorenzo.guazzelli@unipi.it.
  • Mezzetta A; Dipartimento di Farmacia, Università di Pisa Via Bonanno 33 56126 Pisa Italy cinzia.chiappe@unipi.it lorenzo.guazzelli@unipi.it.
  • Guazzelli L; Dipartimento di Farmacia, Università di Pisa Via Bonanno 33 56126 Pisa Italy cinzia.chiappe@unipi.it lorenzo.guazzelli@unipi.it.
  • Sartini S; Dipartimento di Farmacia, Università di Pisa Via Bonanno 33 56126 Pisa Italy cinzia.chiappe@unipi.it lorenzo.guazzelli@unipi.it.
  • Pomelli CS; Dipartimento di Farmacia, Università di Pisa Via Bonanno 33 56126 Pisa Italy cinzia.chiappe@unipi.it lorenzo.guazzelli@unipi.it.
  • Parker WO; Eni, Research & Technical Innovation, Physical Chemistry Department Via Maritano 26, San Donato Milanese 20097 Italy.
  • Chiappe C; Dipartimento di Farmacia, Università di Pisa Via Bonanno 33 56126 Pisa Italy cinzia.chiappe@unipi.it lorenzo.guazzelli@unipi.it.
RSC Adv ; 8(38): 21174-21183, 2018 Jun 08.
Article en En | MEDLINE | ID: mdl-35539901
Supported chiral ionic liquids (SILs) were prepared choosing the starting material for the ionic liquid part from the enantiopure stock of the chiral pool (monoterpenoids and an amino acid) and the sporopollenin as an environmentally friendly support. Sporopollenins are microcapsules with naturally well-defined sizes and shapes that can be obtained from pollen grains after removal of the internal cytoplasm and the second shell layer. As thermally stable organic biocompatible structures, sporopollenins have attracted increasing interest in recent years for several applications. Herein, bio-based ILs were anchored onto the surface of sporopollenins obtained from the pollen of Populus deltoides, selected as a model pollen grain. These new structures, which present an external positively charged shell, were characterized by physico-chemical techniques (ATR-FTIR, TGA, SEM, EDX, and solid-state 13C NMR). A metathesis reaction was also performed on selected bio-based IL modified sporopollenins, demonstrating the possibility to switch the surface properties by exploiting well-known IL chemistry.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: RSC Adv Año: 2018 Tipo del documento: Article Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: RSC Adv Año: 2018 Tipo del documento: Article Pais de publicación: Reino Unido