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Recent advances in catalytic chain transfer polymerization of isobutylene: a review.
Rajasekhar, Tota; Singh, Gurmeet; Kapur, Gurpreet Singh; Ramakumar, S S V.
Afiliación
  • Rajasekhar T; R&D Center, Indian Oil Corporation Limited Sector-13 Faridabad-121007 Haryana India rajasekhart@indianoil.in kapurgs@indianoil.in.
  • Singh G; R&D Center, Indian Oil Corporation Limited Sector-13 Faridabad-121007 Haryana India rajasekhart@indianoil.in kapurgs@indianoil.in.
  • Kapur GS; R&D Center, Indian Oil Corporation Limited Sector-13 Faridabad-121007 Haryana India rajasekhart@indianoil.in kapurgs@indianoil.in.
  • Ramakumar SSV; R&D Center, Indian Oil Corporation Limited Sector-13 Faridabad-121007 Haryana India rajasekhart@indianoil.in kapurgs@indianoil.in.
RSC Adv ; 10(31): 18180-18191, 2020 May 10.
Article en En | MEDLINE | ID: mdl-35517218
This review presents the development of highly reactive polyisobutylene (HRPIB), a major commercial intermediate toward fuel and lubricant additives. Recent years have witnessed very substantial advances in the catalytic chain transfer polymerization (CCTP) of isobutylene/industrial Raffinate-1 (C4 Raffinate) to produce HRPIB, particularly in nonpolar solvents at elevated temperatures. The main subjects of this review are cationic polymerization of isobutylene, progress in HRPIB research and existing challenges, and recent advances of CCTP. New initiating/catalyst systems based on ionic liquids with Lewis acids are detailed, and this approach may open new views in the synthesis of HRPIB. Some current developments in CCTP of industrial Raffinate-1 and mechanistic studies are also described. This review strongly supports that the hydrocarbon soluble Lewis acid·ether (LA·ether) complex catalyzed CCTP will become the most popular technique for preparing HRPIB and could replace the traditional BF3 catalyzed industrial method.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: RSC Adv Año: 2020 Tipo del documento: Article Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: RSC Adv Año: 2020 Tipo del documento: Article Pais de publicación: Reino Unido