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A first look at the N- and O-glycosylation landscape in anuran skin secretions.
Barbosa, Eder Alves; Alves, Gabriel Sérgio Costa; Coura, Marcelo de Melo Andrade; Silva, Higor de Lima E; Rocha, Filipe Souza da; Nunes, João Bueno; Watanabe, Matheus de Souza; Andrade, Alan Carvalho; Brand, Guilherme Dotto.
Afiliación
  • Barbosa EA; Laboratório de Síntese e Análise de Biomoléculas - LSAB, Instituto de Química - IQ, Universidade de Brasília - UnB, Brasília, DF, Brazil; Laboratório de Espectrometria de Massa - LEM, Embrapa Recursos Genéticos e Biotecnologia, Brasília, DF, Brazil.
  • Alves GSC; Laboratório de Processos Biológicos e Ativos Biotecnológicos - LPBAB, Instituto de Ciências Biológicas - IB, Universidade de Brasília - UnB, Brasília, DF, Brazil.
  • Coura MMA; Divisão de Cirurgia Colorretal, Hospital Universitário de Brasília, Escola de Medicina, Universidade de Brasília - UnB, Brasília, DF, Brazil.
  • Silva HLE; Laboratório de Síntese e Análise de Biomoléculas - LSAB, Instituto de Química - IQ, Universidade de Brasília - UnB, Brasília, DF, Brazil.
  • Rocha FSD; Laboratório de Síntese e Análise de Biomoléculas - LSAB, Instituto de Química - IQ, Universidade de Brasília - UnB, Brasília, DF, Brazil.
  • Nunes JB; Laboratório de Síntese e Análise de Biomoléculas - LSAB, Instituto de Química - IQ, Universidade de Brasília - UnB, Brasília, DF, Brazil.
  • Watanabe MS; Laboratório de Síntese e Análise de Biomoléculas - LSAB, Instituto de Química - IQ, Universidade de Brasília - UnB, Brasília, DF, Brazil.
  • Andrade AC; Universidade Federal de Lavras, Campus UFLA, Lavras, MG, 37200-000, Brazil; Embrapa Café, INOVACAFÉ, Campus UFLA, Lavras, MG, 37200-000, Brazil.
  • Brand GD; Laboratório de Síntese e Análise de Biomoléculas - LSAB, Instituto de Química - IQ, Universidade de Brasília - UnB, Brasília, DF, Brazil. Electronic address: gdbrand@unb.br.
Biochimie ; 197: 19-37, 2022 Jun.
Article en En | MEDLINE | ID: mdl-35077806
Amphibians secrete a complex array of molecules that shape their interactions with coinhabiting microorganisms and macroscopic predators. Glycans are a rapidly evolving and complex class of biomolecules implicated in intrinsic and extrinsic recognition events. Despite the numerous studies aiming at the biochemical characterization of anuran skin secretions, little is known about protein-linked oligosaccharides, their synthesis pathways, and their homing secreted glycoproteins. In the present report, LC-MS/MS was used to investigate the diversity of N- and O-linked oligosaccharides in the skin secretion of two South American frogs, Pithecopus azureus and Boana raniceps. Additionally, the enzymes responsible for glycan synthesis pathways were evaluated based on their skin tissue transcriptome. Our analyses allowed the annotation of various N- and O-glycan structures commonly found in vertebrate proteins. Paucimannosidic glycans were abundant in the skin secretion of both amphibians; however, hybrid and complex N-glycan structures were detected only in B. raniceps. A good correlation between the structures discovered in glycomic analyses and transcripts encoding enzymes necessary for their synthesis was obtained. Some transcripts such as those of MAN1A2, FUT8, and ST6GALNAC were found solely in B. raniceps. Finally, secreted N- and O- linked glycoproteins were predicted from the transcriptomic data, indicating that proteases and protease inhibitors are putative sources of the glycans described herein. Overall, our results show the presence of oligosaccharides in amphibians skin secretions and suggest that their diversity is species-specific, paving the way for novel perspectives involving amphibian evolution and ecology.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Glicoproteínas / Espectrometría de Masas en Tándem Límite: Animals Idioma: En Revista: Biochimie Año: 2022 Tipo del documento: Article País de afiliación: Brasil Pais de publicación: Francia

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Glicoproteínas / Espectrometría de Masas en Tándem Límite: Animals Idioma: En Revista: Biochimie Año: 2022 Tipo del documento: Article País de afiliación: Brasil Pais de publicación: Francia