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Characterizing Anion Adsorption to Aqueous Interfaces: Toluene-Water versus Air-Water.
Devlin, Shane W; McCaffrey, Debra L; Saykally, Richard J.
Afiliación
  • Devlin SW; Department of Chemistry, University of California, Berkeley, California 94720, United States.
  • McCaffrey DL; Chemical Sciences Division, Lawrence Berkeley National Lab, Berkeley, California 94720, United States.
  • Saykally RJ; Department of Chemistry, University of California, Berkeley, California 94720, United States.
J Phys Chem Lett ; 13(1): 222-228, 2022 Jan 13.
Article en En | MEDLINE | ID: mdl-34967638
We continue our investigation of the behavior of simple ions at aqueous interfaces, employing the combination of two surface-sensitive nonlinear spectroscopy tools, broadband deep UV electronic sum-frequency generation and UV second harmonic generation, to characterize the adsorption of thiocyanate to the interface of water with toluene─a prototypical hydrophobe. We find that both the interfacial spectrum and the Gibbs free energy of adsorption closely match results previously reported for the air-water interface. We observe no relative spectral shift in the higher-energy CTTS transition of thiocyanate, implying similar solvation environments for the two interfaces. Similarly, the Gibbs free energies of adsorption agree within error; however, we expect the respective enthalpic and entropic contributions to differ between the two interfaces, similar to our earlier findings for the air-water versus graphene-water interfaces. Further experiments and theoretical modeling are necessary to quantify the mechanistic differences.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Prognostic_studies Idioma: En Revista: J Phys Chem Lett Año: 2022 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Prognostic_studies Idioma: En Revista: J Phys Chem Lett Año: 2022 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos