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The Chosen Few: Parallel Library Reaction Methodologies for Drug Discovery.
Dombrowski, Amanda W; Aguirre, Ana L; Shrestha, Anurupa; Sarris, Kathy A; Wang, Ying.
Afiliación
  • Dombrowski AW; Advanced Chemistry Technologies Group, AbbVie, Inc., North Chicago, Illinois 60064, United States.
  • Aguirre AL; Advanced Chemistry Technologies Group, AbbVie, Inc., North Chicago, Illinois 60064, United States.
  • Shrestha A; Advanced Chemistry Technologies Group, AbbVie, Inc., North Chicago, Illinois 60064, United States.
  • Sarris KA; Advanced Chemistry Technologies Group, AbbVie, Inc., North Chicago, Illinois 60064, United States.
  • Wang Y; Advanced Chemistry Technologies Group, AbbVie, Inc., North Chicago, Illinois 60064, United States.
J Org Chem ; 87(4): 1880-1897, 2022 02 18.
Article en En | MEDLINE | ID: mdl-34780177
Parallel library synthesis is an important tool for drug discovery because it enables the synthesis of closely related analogues in parallel via robust and general synthetic transformations. In this perspective, we analyzed the synthetic methodologies used in >5000 parallel libraries representing 15 prevalent synthetic transformations. The library data set contains complex substrates and diverse arrays of building blocks used over the last 14 years at AbbVie. The library synthetic methodologies that have demonstrated robustness and generality with proven success are described along with their substrate scopes. The evolution of the synthetic methodologies for library synthesis over the past decade is discussed. We also highlight that the combination of parallel library synthesis with high-throughput experimentation will continue to facilitate the discovery of library-amenable synthetic methodologies in drug discovery.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Descubrimiento de Drogas Idioma: En Revista: J Org Chem Año: 2022 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Descubrimiento de Drogas Idioma: En Revista: J Org Chem Año: 2022 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Estados Unidos