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Hydroxycinnamic acid-spermidine amides from Tetragonisca angustula honey as anti-Neospora caninum: In vitro and in silico studies.
Lima, Ângela C de O; Conceição, Rodrigo S; Freitas, Luciana S; de Carvalho, Carlos A L; Conceição, Antônio L da S; Freitas, Humberto F; Pita, Samuel S da R; Ifa, Demian R; Pinheiro, Alexandre M; Branco, Alexsandro.
Afiliación
  • Lima ÂCO; Graduate Program in Biotechnology, State University of Feira de Santana - UEFS, Feira de Santana, Brazil.
  • Conceição RS; Veterinary, Biochemistry and Immunology Laboratory, Center for Agricultural, Environmental and Biological Sciences, Federal University of Reconcavo da Bahia, Cruz das Almas, Brazil.
  • Freitas LS; Graduate Program in Biotechnology, State University of Feira de Santana - UEFS, Feira de Santana, Brazil.
  • de Carvalho CAL; Veterinary, Biochemistry and Immunology Laboratory, Center for Agricultural, Environmental and Biological Sciences, Federal University of Reconcavo da Bahia, Cruz das Almas, Brazil.
  • Conceição ALDS; Center for Agricultural, Environmental and Biological Sciences, Federal University of Reconcavo da Bahia, Cruz das Almas, Brazil.
  • Freitas HF; Center for Agricultural, Environmental and Biological Sciences, Federal University of Reconcavo da Bahia, Cruz das Almas, Brazil.
  • Pita SSDR; Laboratory of Bioinformatics and Molecular Modeling (LaBiMM), Pharmacy College, Federal University of Bahia (UFBA), Salvador, Brazil.
  • Ifa DR; Laboratory of Bioinformatics and Molecular Modeling (LaBiMM), Pharmacy College, Federal University of Bahia (UFBA), Salvador, Brazil.
  • Pinheiro AM; Department of Chemistry, Center for Research in Mass Spectrometry, York University, Toronto, Ontario, Canada.
  • Branco A; Veterinary, Biochemistry and Immunology Laboratory, Center for Agricultural, Environmental and Biological Sciences, Federal University of Reconcavo da Bahia, Cruz das Almas, Brazil.
Chem Biol Drug Des ; 98(6): 1104-1115, 2021 12.
Article en En | MEDLINE | ID: mdl-34614302
Tetragonisca angustula honey was fractioned in a SiO2 column to furnish three fractions (A-C) in which four hydroxycinnamic acid-Spermidine amides (HCAAs), known as N', N″, N‴-tris-p-coumaroyl spermidine, N', N″-dicaffeoyl, N‴-coumaroyl spermidine, N', N″, N‴-tris-caffeoyl spermidine and N', N″-dicaffeoyl and N‴-feruloyl spermidine were identified in the fractions B and C by electrospray ionization tandem mass spectrometry. A primary culture model previously infected with Neospora caninum (72 h) was used to evaluate the honey fractions (A-C) for two-time intervals: 24 and 72 h. Parasitic reduction ranged from 38% on fraction C (12.5 µg/ml), after 24 h, to 54% and 41% with fractions B and C (25 µg/ml) after 72 h of treatment, respectively. Additionally, HCAAs did not show any cell toxicity for 24 and 72 h. For infected cultures (72 h), the active fractions B (12.5 µg/ml) and C (25 µg/ml) decreased their NO content. In silico studies suggest that HCAAs may affect the parasite's redox pathway and improve the oxidative effect of NO released from infected cells. Here, we presented for the first time, that HCAAs from T. angustula honey have the potential to inhibit the growth of N. caninum protozoa.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Abejas / Espermidina / Neospora / Miel / Antiprotozoarios Límite: Animals País/Región como asunto: America do sul / Brasil Idioma: En Revista: Chem Biol Drug Des Asunto de la revista: BIOQUIMICA / FARMACIA / FARMACOLOGIA Año: 2021 Tipo del documento: Article País de afiliación: Brasil Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Abejas / Espermidina / Neospora / Miel / Antiprotozoarios Límite: Animals País/Región como asunto: America do sul / Brasil Idioma: En Revista: Chem Biol Drug Des Asunto de la revista: BIOQUIMICA / FARMACIA / FARMACOLOGIA Año: 2021 Tipo del documento: Article País de afiliación: Brasil Pais de publicación: Reino Unido