Your browser doesn't support javascript.
loading
Liquid chromatography-tandem mass spectrometry analysis for identification and quantification of antimicrobial compounds in distillery wastewater.
Hou, Waner; Ling, Jiayin; Xu, Yanbin; Li, Kailing; Wang, Fei.
Afiliación
  • Hou W; Analysis and Test Center, Guangdong University of Technology, Guangzhou 510006, China.
  • Ling J; Guangdong Provincial Key Laboratory of Environmental Health and Land Resource, Zhaoqing University, Zhaoqing 526061, Guangdong, China.
  • Xu Y; School of Environmental Science and Engineering, Guangdong University of Technology, Guangzhou 510006, China.
  • Li K; Analysis and Test Center, Guangdong University of Technology, Guangzhou 510006, China.
  • Wang F; School of Environmental Science and Engineering, Guangdong University of Technology, Guangzhou 510006, China.
MethodsX ; 8: 101470, 2021.
Article en En | MEDLINE | ID: mdl-34430343
A high-resolution mass spectrometry (HR-MS) method was developed to analyze and identify small molecule compounds in distillery wastewater. According to identification confidence levels, 4 levels of compounds were identified. The five antimicrobial compounds (lactic acid, succinic acid, acetophenone, cinnamic acid, and phenyllactic acid), which shown in high concentrations, were at the highest level of confidence (level 1, confirmed structure). Thus, a rapid and sensitive liquid chromatography-tandem mass spectrometry (LC-MS/MS) method was developed to simultaneously quantify these antimicrobial compounds. The analysis was performed in the selective reaction monitoring (SRM) mode via the electrospray ionization (ESI) source operating in the negative ionization mode. Linear calibration curves were obtained over the concentration range of 50-1000.0 ng/mL for succinic acid, acetophenone, cinnamic acid, phenyllactic acid, and 375-7500 ng/mL for lactic acid. Precision and recovery of the analytes were all satisfactory (relative standard deviation < 10%). The validated method was successfully applied to quantitative analysis of the five antimicrobial compounds in distillery wastewater.•Analyze and identify 4 levels of small molecule compounds in distillery wastewater.•Simple method for quantification of five antimicrobial compounds.•Column temperature affected the lactic and succinic acid chromatographs significantly.
Palabras clave
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
Buscar en Google

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: MethodsX Año: 2021 Tipo del documento: Article País de afiliación: China Pais de publicación: Países Bajos
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
Buscar en Google

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: MethodsX Año: 2021 Tipo del documento: Article País de afiliación: China Pais de publicación: Países Bajos