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Crystal structure of potassium hydrogen bis-((E)-2-{4-[3-(thio-phen-3-yl)acrylo-yl]phen-oxy}acetate).
Vu Quoc, Trung; Phan Thuy, Linh; Do Ba, Dai; Tran Thi Thuy, Duong; Nguyen Ngoc, Linh; Nguyen Thuy, Chinh; Duong Khanh, Linh; Ha Manh, Hung; Thai, Hoang; Le Van, Khoe; Van Meervelt, Luc.
Afiliación
  • Vu Quoc T; Faculty of Chemistry, Hanoi National University of Education, 136 Xuan Thuy, Cau Giay, Hanoi 10000, Vietnam.
  • Phan Thuy L; High School for Gifted Students, Hanoi National University of Education, 136 Xuan Thuy, Cau Giay, Hanoi 10000, Vietnam.
  • Do Ba D; Nguyen Trai High School, 50 Nam Cao Street, Ba Dinh, Hanoi 10000, Vietnam.
  • Tran Thi Thuy D; Bien Hoa Gifted High School, 86 Chu Van An Street, Phu Ly City, Ha Nam Province, Vietnam.
  • Nguyen Ngoc L; Faculty of Training Bachelor of Practice, Than Do University, Kim Chung, Hoai Duc, Hanoi 10000, Vietnam.
  • Nguyen Thuy C; Institute of Tropical Technology, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet, Cau Giay, Hanoi 10000, Vietnam.
  • Duong Khanh L; Graduate University of Science and Technology, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet, Cau Giay, Hanoi 10000, Vietnam.
  • Ha Manh H; Faculty of Chemistry, Hanoi National University of Education, 136 Xuan Thuy, Cau Giay, Hanoi 10000, Vietnam.
  • Thai H; Faculty of General Education, Hanoi University of Mining and Geology, Duc Thang Ward, Bac Tu Liem District, Hanoi 10000, Vietnam.
  • Le Van K; Institute of Tropical Technology, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet, Cau Giay, Hanoi 10000, Vietnam.
  • Van Meervelt L; Graduate University of Science and Technology, Vietnam Academy of Science and Technology, 18 Hoang Quoc Viet, Cau Giay, Hanoi 10000, Vietnam.
Acta Crystallogr E Crystallogr Commun ; 77(Pt 6): 609-614, 2021 Jun 01.
Article en En | MEDLINE | ID: mdl-34164137
The synthesis and spectroscopic data of (E)-2-{4-[3-(thio-phen-3-yl)acrylo-yl]phen-oxy}acetic acid are described. Crystallization from an ethanol-water mixture resulted in the title compound, C30H23KO8S2 or [K(C15H11O4S)(C15H12O4S)] n , containing one mol-ecule of the acid and one mol-ecule of the potassium salt in the asymmetric unit. Both mol-ecules share the H atom between their carboxyl groups and a potassium ion. The C=C bonds display an E configuration. The thio-phene and phenyl rings in the two mol-ecules are inclined by 43.3 (2) and 22.7 (2)°. The potassium ion is octa-hedrally coordinated by six O atoms. This distorted octa-hedron shares on opposite sides two oxygen atoms with inversion-related octa-hedra, resulting in chains of octa-hedra running in the [010] direction, which form ladder-like chains by C-H⋯π inter-actions. A Hirshfeld surface analysis indicates that the highest contributions to the surface contacts arise from inter-actions in which H atoms are involved, with the most important contribution being from H⋯H (31.6 and 31.9% for the two mol-ecules) inter-actions.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Acta Crystallogr E Crystallogr Commun Año: 2021 Tipo del documento: Article País de afiliación: Vietnam Pais de publicación: Reino Unido
Texto completo
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Imprimir
XML
PubMed Links
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Acta Crystallogr E Crystallogr Commun Año: 2021 Tipo del documento: Article País de afiliación: Vietnam Pais de publicación: Reino Unido