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Design of turn-on luminescent sensor based on nanostructured molecularly imprinted polymer-coated zirconium metal-organic framework for selective detection of chloramphenicol residues in milk and honey.
Amiripour, Fatemeh; Ghasemi, Shahram; Azizi, Seyed Naser.
Afiliación
  • Amiripour F; Analytical Division, Faculty of Chemistry, University of Mazandaran, 47416-95447 Babolsar, Iran.
  • Ghasemi S; Faculty of Chemistry, University of Mazandaran, Babolsar, Iran. Electronic address: sghasemi@umz.ac.ir.
  • Azizi SN; Analytical Division, Faculty of Chemistry, University of Mazandaran, 47416-95447 Babolsar, Iran.
Food Chem ; 347: 129034, 2021 Jun 15.
Article en En | MEDLINE | ID: mdl-33486363
Herein, an optical sensor based on nanostructured molecularly imprinted polymer (MIP) coated on a luminescent zirconium metal-organic framework (MIP/Zr-LMOF) is introduced, and its performance is investigated for the fluorescent determination of chloramphenicol (CAP) antibiotic residues in milk and honey. To fabricate the sensor, the surface of Zr-LMOF is modified with MIP in the presence of CAP template, resulting in the introduction of recognition sites for antibiotic molecules. The porous structure of Zr-LMOF with specific binding sites for CAP recognition benefiting from coated MIP leads to selective and sensitive detection of antibiotic. The probe yields a linear range for detection of CAP in trace concentrations (0.16-161.56 µg.L-1) and provides a detection limit of 0.013 µg.L-1. Acceptable recoveries are achieved for antibiotic in real samples, which are consistent with that obtained from liquid chromatography-tandem mass spectrometry (LC-MS/MS), confirm the favorable performance of sensor for accurate determination of CAP in practical applications.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Circonio / Cloranfenicol / Leche / Nanoestructuras / Estructuras Metalorgánicas / Polímeros Impresos Molecularmente / Miel Tipo de estudio: Diagnostic_studies Límite: Animals Idioma: En Revista: Food Chem Año: 2021 Tipo del documento: Article País de afiliación: Irán Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Circonio / Cloranfenicol / Leche / Nanoestructuras / Estructuras Metalorgánicas / Polímeros Impresos Molecularmente / Miel Tipo de estudio: Diagnostic_studies Límite: Animals Idioma: En Revista: Food Chem Año: 2021 Tipo del documento: Article País de afiliación: Irán Pais de publicación: Reino Unido