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Waveguide-based surface-enhanced Raman spectroscopy detection of protease activity using non-natural aromatic amino acids.
Turk, Nina; Raza, Ali; Wuytens, Pieter; Demol, Hans; Daele, Michiel Van; Detavernier, Christophe; Skirtach, Andre; Gevaert, Kris; Baets, Roel.
Afiliación
  • Turk N; Photonics Research Group, Ghent University - IMEC, Technologiepark 126, 9052 Ghent, Belgium.
  • Raza A; Center for Nano- and Biophotonics, Ghent, Belgium.
  • Wuytens P; Photonics Research Group, Ghent University - IMEC, Technologiepark 126, 9052 Ghent, Belgium.
  • Demol H; Center for Nano- and Biophotonics, Ghent, Belgium.
  • Daele MV; Currently with Microsoft, Keilalahdentie 2-4, 02150 Espoo, Finland.
  • Detavernier C; Photonics Research Group, Ghent University - IMEC, Technologiepark 126, 9052 Ghent, Belgium.
  • Skirtach A; Center for Nano- and Biophotonics, Ghent, Belgium.
  • Gevaert K; Currently with IMEC, Kapeldreef 75, 3001 Heverlee, Belgium.
  • Baets R; VIB-UGent Center for Medical Biotechnology, Ghent, Belgium.
Biomed Opt Express ; 11(8): 4800-4816, 2020 Aug 01.
Article en En | MEDLINE | ID: mdl-32923079
Surface enhanced Raman spectroscopy (SERS) is a selective and sensitive technique, which allows for the detection of protease activity by monitoring the cleavage of peptide substrates. Commonly used free-space based SERS substrates, however, require the use of bulky and expensive instrumentation, limiting their use to laboratory environments. An integrated photonics approach aims to implement various free-space optical components to a reliable, mass-reproducible and cheap photonic chip. We here demonstrate integrated SERS detection of trypsin activity using a nanoplasmonic slot waveguide as a waveguide-based SERS substrate. Despite the continuously improving SERS performance of the waveguide-based SERS substrates, they currently still do not reach the SERS enhancements of free-space substrates. To mitigate this, we developed an improved peptide substrate in which we incorporated the non-natural aromatic amino acid 4-cyano-phenylalanine, which provides a high intrinsic SERS signal. The use of non-natural aromatics is expected to extend the possibilities for multiplexing measurements, where the activity of several proteases can be detected simultaneously.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: Biomed Opt Express Año: 2020 Tipo del documento: Article País de afiliación: Bélgica Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: Biomed Opt Express Año: 2020 Tipo del documento: Article País de afiliación: Bélgica Pais de publicación: Estados Unidos