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Assessment of sulfonated homo and co-polyimides incorporated polysulfone ultrafiltration blend membranes for effective removal of heavy metals and proteins.
Jafar Mazumder, Mohammad A; Raja, Panchami H; Isloor, Arun M; Usman, Muhammad; Chowdhury, Shakhawat H; Ali, Shaikh A; Al-Ahmed, Amir.
Afiliación
  • Jafar Mazumder MA; Chemistry Department, King Fahd University of Petroleum & Minerals, Dhahran, 31261, Saudi Arabia. jafar@kfupm.edu.sa.
  • Raja PH; Membrane Technology Laboratory, Chemistry Department, National Institute of Technology Karnataka, Surathkal, Mangalore, 575 025, India.
  • Isloor AM; Membrane Technology Laboratory, Chemistry Department, National Institute of Technology Karnataka, Surathkal, Mangalore, 575 025, India.
  • Usman M; Center for Research Excellence in Nanotechnology (CENT), King Fahd University of Petroleum & Minerals, Dhahran, 31261, Saudi Arabia.
  • Chowdhury SH; Department of Civil and Environmental Engineering, King Fahd University of Petroleum & Minerals, Dhahran, 31261, Saudi Arabia.
  • Ali SA; Chemistry Department, King Fahd University of Petroleum & Minerals, Dhahran, 31261, Saudi Arabia.
  • Inamuddin; Chemistry Department, Faculty of Science, King Abdulaziz University, Jeddah 21589, Saudi Arabia.
  • Al-Ahmed A; Advanced Functional Materials Laboratory, Department of Applied Chemistry, Faculty of Engineering and Technology, Aligarh Muslim University, Aligarh, 202 002, India.
Sci Rep ; 10(1): 7049, 2020 04 27.
Article en En | MEDLINE | ID: mdl-32341422
Sulfonated homo and co- polyimide (sPI) were synthesized with new compositional ratios, and used as additives (0.5 wt%, 0.75 wt%, and 1.0 wt%) to prepare blend membranes with polysulfone (PSf). Flat sheet membranes for ultrafiltration (UF) were casted using the phase inversion technique. Surface morphology of the prepared UF membranes were characterized by atomic force microscopy (AFM) and scanning electron microscopy (SEM). Surface charge of the membranes were determined by zeta potential, and hydrophilicity was studied by contact angle measurement. The contact angle of the membrane decreased with increasing sPI additive indicates increasing the hydrophilicity of the blend membranes. Filtration studies were conducted for rejection of heavy metals (Pb2+ and Cd2+) and proteins (pepsin and BSA). Blend membranes showed better rejection than pure PSf membrane. Among the blend membranes it was observed that with increasing amount of sPIs enhance the membrane properties and finally, PSf-sPI5 membrane with 1 wt% of sPI5 showed the improved permeability (72.1 L m-2 h-1 bar-1), and the best rejection properties were found for both metal ions (≈98% of Pb2+; ≈92% of Cd2+) and proteins (>98% of BSA; > 86% of Pepsin). Over all, this membrane was having better hydrophilicity, porosity and higher number of sites to attach the metal ions. Its performance was even better than several-reported sulfonic acid based UF membranes. All these intriguing properties directed this new UF membrane for its potential application in wastewater treatment.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Sci Rep Año: 2020 Tipo del documento: Article País de afiliación: Arabia Saudita Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Sci Rep Año: 2020 Tipo del documento: Article País de afiliación: Arabia Saudita Pais de publicación: Reino Unido