Your browser doesn't support javascript.
loading
Impact of Co2+ Substitution on Microstructure and Magnetic Properties of CoxZn1-xFe2O4 Nanoparticles.
Mohamed, W S; Alzaid, Meshal; Abdelbaky, Mohammed S M; Amghouz, Zakariae; García-Granda, Santiago; Abu-Dief, Ahmed M.
Afiliación
  • Mohamed WS; Physics Department, College of Science, Jouf University, Al-Jouf, Sakaka P.O. Box 2014, Saudi Arabia.
  • Alzaid M; Physics Department, Faculty of Science, Sohag University, 82524 Sohag, Egypt.
  • Abdelbaky MSM; Physics Department, College of Science, Jouf University, Al-Jouf, Sakaka P.O. Box 2014, Saudi Arabia.
  • Amghouz Z; Departments of Physical and Analytical Chemistry, and Organic and Inorganic Chemistry, University of Oviedo-CINN, 33006 Oviedo, Spain.
  • García-Granda S; Department of Materials Science and Metallurgical Engineering, University of Oviedo, Campus Universitario, 33203 Gijón, Spain.
  • Abu-Dief AM; Departments of Physical and Analytical Chemistry, and Organic and Inorganic Chemistry, University of Oviedo-CINN, 33006 Oviedo, Spain.
Nanomaterials (Basel) ; 9(11)2019 Nov 11.
Article en En | MEDLINE | ID: mdl-31718062
In the present work, we synthesized CoxZn1-xFe2O4 spinel ferrite nanoparticles (x= 0, 0.1, 0.2, 0.3 and 0.4) via the precipitation and hydrothermal-joint method. Structural parameters were cross-verified using X-ray powder diffraction (XRPD) and electron microscopy-based techniques. The magnetic parameters were determined by means of vibrating sample magnetometry. The as-synthesized CoxZn1-xFe2O4 nanoparticles exhibit high phase purity with a single-phase cubic spinel-type structure of Zn-ferrite. The microstructural parameters of the samples were estimated by XRD line profile analysis using the Williamson-Hall approach. The calculated grain sizes from XRPD analysis for the synthesized samples ranged from 8.3 to 11.4 nm. The electron microscopy analysis revealed that the constituents of all powder samples are spherical nanoparticles with proportions highly dependent on the Co doping ratio. The CoxZn1-xFe2O4 spinel ferrite system exhibits paramagnetic, superparamagnetic and weak ferromagnetic behavior at room temperature depending on the Co2+ doping ratio, while ferromagnetic ordering with a clear hysteresis loop is observed at low temperatures (5K). We concluded that replacing Zn2+ ions with Co2+ ions changes both the structural and magnetic properties of ZnFe2O4 nanoparticles.
Palabras clave
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
Buscar en Google

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Nanomaterials (Basel) Año: 2019 Tipo del documento: Article País de afiliación: Arabia Saudita Pais de publicación: Suiza
Texto completo
Añadir a Mi BVS
Imprimir
XML
PubMed Links
Buscar en Google

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Nanomaterials (Basel) Año: 2019 Tipo del documento: Article País de afiliación: Arabia Saudita Pais de publicación: Suiza