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Synthesis and anti-cancer activities of glycosides and glycoconjugates of diterpenoid isosteviol.
Sharipova, Radmila R; Belenok, Mayya G; Garifullin, Bulat F; Sapunova, Anastasiya S; Voloshina, Alexandra D; Andreeva, Olga V; Strobykina, Irina Yu; Skvortsova, Polina V; Zuev, Yuriy F; Kataev, Vladimir E.
Afiliación
  • Sharipova RR; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Belenok MG; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Garifullin BF; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Sapunova AS; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Voloshina AD; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Andreeva OV; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Strobykina IY; Arbuzov Institute of Organic and Physical Chemistry , FRC Kazan Scientific Center , Russian Academy of Sciences , Arbuzov str., 8 , Kazan , 420088 , Russian Federation . Email: radmila_sharipov@mail.ru.
  • Skvortsova PV; Kazan Institute of Biochemistry and Biophysics , FRC Kazan Scientific Center , Russian Academy of Sciences , Lobachevsky Str., 2/31 , Kazan , 420111 , Russian Federation.
  • Zuev YF; Kazan Institute of Biochemistry and Biophysics , FRC Kazan Scientific Center , Russian Academy of Sciences , Lobachevsky Str., 2/31 , Kazan , 420111 , Russian Federation.
  • Kataev VE; Kazan State Power Engineering University , 51, Krasnoselskaya str. , Kazan , 420066 , Russian Federation.
Medchemcomm ; 10(8): 1488-1498, 2019 Aug 01.
Article en En | MEDLINE | ID: mdl-31673312
A series of glycosides and glycoconjugates of diterpenoid isosteviol (16-oxo-ent-beyeran-19-oic acid) with various monosaccharide residues were synthesized and their cytotoxicity against some human cancer and normal cell lines was assayed. Most of the synthesized compounds demonstrated moderate to significant cytotoxicity against human cancer cell lines M-HeLa and MCF-7. Three lead compounds exhibited selective cytotoxic activities against M-HeLa (IC50 = 10.0-15.1 µM) that were three times better than the cytotoxicity of the anti-cancer drug Tamoxifen (IC50 = 28.0 µM). Moreover, the lead compounds were not cytotoxic with respect to the normal human cell line Chang liver (IC50 > 100 µM), whereas Tamoxifen inhibited the viability of normal human Chang liver cells with an IC50 value of 46.0 µM. It was determined that the cytotoxicity of the lead compounds was due to induction of apoptosis proceeding along the mitochondrial pathway. The cytotoxic activity of the synthesized compounds substantially depended on the nature of the monosaccharide residue and its position, that is, whether the monosaccharide residue was attached directly to the isosteviol skeleton or was moved away from it by means of a polymethylene linker.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Medchemcomm Año: 2019 Tipo del documento: Article Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Medchemcomm Año: 2019 Tipo del documento: Article Pais de publicación: Reino Unido