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Structure-antifungal relationships and preventive effects of 1-(2,4-dihydroxyphenyl)-2-methylpropan-1-one derivatives as potential inhibitors of class-II fructose-1,6-bisphosphate aldolase.
Luong, Tuong Thi Mai; Wang, Wei-Wei; Zhang, Fan; Dan, Wen-Jia; Nien, Hoang Xuan; Zhang, An-Ling; Li, Ding; Gao, Jin-Ming.
Afiliación
  • Luong TTM; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China; Faculty of Basic Science, Vietnam National University of F
  • Wang WW; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China.
  • Zhang F; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China.
  • Dan WJ; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China.
  • Nien HX; Institute of Scientific Research and Technological Development, Thu Dau Mot University, Binh Duong, Viet Nam.
  • Zhang AL; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China.
  • Li D; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China. Electronic address: jbolid@nwsuaf.edu.cn.
  • Gao JM; Shaanxi Key Labotory of Natural Products & Chemical Biology, Shaanxi Engineering Center of Bioresource Chemistry & Sustainable Utilization, College of Chemistry & Pharmacy, Northwest A&F University, Yangling 712100, PR China. Electronic address: jinminggao@nwsuaf.edu.cn.
Pestic Biochem Physiol ; 159: 41-50, 2019 Sep.
Article en En | MEDLINE | ID: mdl-31400783
Emerging fungal phytodiseases are a food security threat and novel fungicides are in an urgent need. Herein, a series of isobutyrophenone derivatives were designed and synthesized. The derivatives exhibited excellent fungicidal activities against seven fungi. The structure-activity relationship (SAR) study indicated that the introduction of a bromo group at the position 3 or 5 of the phenyl ring, as well as esterification of the 4-hydroxy with a chloroacetyl group, could substantially increase the antifungal activity and spectrum of the compounds. Among all 23 compounds, 2-bromo-3-hydroxy-4-isobutyryl-6-methylphenyl 2-chloroacetate (12b) showed the highest fungicidal activity against all seven tested fungal pathogens with EC50 values ranging from 1.22 to 39.94 µg/mL and exhibited the most potent inhibition against class II fructose-1,6-bisphosphate aldolase with an IC50 of 3.63 µM. The lead compounds were proven to be safe to NIH3T3/293 T cells and silkworm larvae, and relatively stable under different harsh conditions. Detached fruit tests showed the practical potential of lead compounds for fruit (or plant) protection. Taken together, our results indicated that the isobutyrophenone derivatives could be further optimized and developed as advanced leads for new fungicides.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Fructosa-Bifosfato Aldolasa / Antifúngicos Límite: Animals / Humans Idioma: En Revista: Pestic Biochem Physiol Año: 2019 Tipo del documento: Article Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Fructosa-Bifosfato Aldolasa / Antifúngicos Límite: Animals / Humans Idioma: En Revista: Pestic Biochem Physiol Año: 2019 Tipo del documento: Article Pais de publicación: Estados Unidos