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Optimization of Ultrasound-Assisted Extraction of Phenolic Compounds from Annona muricata By-Products and Pulp.
Aguilar-Hernández, Gabriela; García-Magaña, María de Lourdes; Vivar-Vera, María de Los Ángeles; Sáyago-Ayerdi, Sonia Guadalupe; Sánchez-Burgos, Jorge Alberto; Morales-Castro, Juliana; Anaya-Esparza, Luis Miguel; Montalvo González, Efigenia.
Afiliación
  • Aguilar-Hernández G; Laboratorio de Integral de Investigación de Alimentos, Tecnológico Nacional de México/Instituto Tecnológico de Tepic, Av. Tecnológico 2595, Lagos del Country, Tepic 63175, Mexico. gaby.mca2017@gmail.com.
  • García-Magaña ML; Laboratorio de Integral de Investigación de Alimentos, Tecnológico Nacional de México/Instituto Tecnológico de Tepic, Av. Tecnológico 2595, Lagos del Country, Tepic 63175, Mexico. mgarciam@ittepic.edu.mx.
  • Vivar-Vera MLÁ; Tecnológico Nacional de México/Instituto Tecnológico de Tuxtepec. Depto. de Ingeniería Química y Bioquímica-Maestría en Ciencias en Alimentos, Av. Dr. Víctor Bravo Ahuja S/N. Col. 5 de Mayo, Tuxtepec 68350, Mexico. maryangeles.vivar@gmail.com.
  • Sáyago-Ayerdi SG; Laboratorio de Integral de Investigación de Alimentos, Tecnológico Nacional de México/Instituto Tecnológico de Tepic, Av. Tecnológico 2595, Lagos del Country, Tepic 63175, Mexico. ssayago@ittepic.edu.mx.
  • Sánchez-Burgos JA; Laboratorio de Integral de Investigación de Alimentos, Tecnológico Nacional de México/Instituto Tecnológico de Tepic, Av. Tecnológico 2595, Lagos del Country, Tepic 63175, Mexico. jorgealberto_sanchezburgos@yahoo.com.mx.
  • Morales-Castro J; Departamento de Ingenierías Química y Bioquímica, Tecnológico Nacional de México/Campus-Instituto Tecnológico de Durango, Felipe Pescador 1830 Ote., Durango 34080, Mexico. jmorales@itdurango.edu.mx.
  • Anaya-Esparza LM; Laboratorio de Integral de Investigación de Alimentos, Tecnológico Nacional de México/Instituto Tecnológico de Tepic, Av. Tecnológico 2595, Lagos del Country, Tepic 63175, Mexico. l_m_ae@hotmail.com.
  • Montalvo González E; Laboratorio de Integral de Investigación de Alimentos, Tecnológico Nacional de México/Instituto Tecnológico de Tepic, Av. Tecnológico 2595, Lagos del Country, Tepic 63175, Mexico. emontalvo@ittepic.edu.mx.
Molecules ; 24(5)2019 Mar 05.
Article en En | MEDLINE | ID: mdl-30841508
Ultrasound-assisted extraction (UAE) is widely used; however, the efficiency of extraction depends on the raw materials. Therefore, optimization of UAE must be investigated for each type of plant material. By-products from soursop fruit have not been studied as a source of bioactive compounds. In this work, the optimization of UAE conditions (extraction time (5, 10, and 15 min), pulse cycle (0.4, 0.7, and 1 s), and sonication amplitude (40%, 70%, and 100%)) for the extraction of phenolic compounds (soluble, hydrolyzable, condensed tannins, and total polyphenols) from soursop by-products (seed, peel, and columella) and pulp was evaluated using response surface methodology. The optimal conditions for UAE to obtain the highest total polyphenol content from by-products and pulp was dependent on the raw material. Peel resulted in the highest content of total polyphenols (187.32 mg/g dry matter [DM]) followed by columella (164.14 mg/g DM), seed (36.15 mg/g DM), and pulp (33.24 mg/g DM). The yield of polyphenolic content from peel and columella obtained with UAE was higher (32⁻37%) than conventional extraction for 2 h under stirring (14⁻16%). The contents of gallic acid (0.36⁻15.86 µg/g DM), coumaric acid (0.07⁻1.37 µg/g DM), and chlorogenic acid (9.18⁻32.67 µg/g DM) in the different parts of the fruit were higher in the extracts obtained by UAE compared with a conventional extraction method (0.08⁻0.61, 0.05⁻0.08, 3.15⁻13.08 µg/g DM, respectively), although it was dependent on the raw materials. Soursop by-products can be functionally important if they are used to extract bioactive compounds by UAE; a technology with high potential for commercial extraction on a large scale.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Fenoles / Sonicación / Extractos Vegetales / Annona / Fraccionamiento Químico Idioma: En Revista: Molecules Asunto de la revista: BIOLOGIA Año: 2019 Tipo del documento: Article País de afiliación: México Pais de publicación: Suiza

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Fenoles / Sonicación / Extractos Vegetales / Annona / Fraccionamiento Químico Idioma: En Revista: Molecules Asunto de la revista: BIOLOGIA Año: 2019 Tipo del documento: Article País de afiliación: México Pais de publicación: Suiza