Efficient extraction and characterization of pectin from orange peel by a combined surfactant and microwave assisted process.
Food Chem
; 286: 1-7, 2019 Jul 15.
Article
en En
| MEDLINE
| ID: mdl-30827581
Surfactant and microwave assisted extraction (S-MAE) was used for pectin extraction from orange peel. First, we optimized the conditions of microwave assisted extraction (MAE), e.g., irradiation time, liquid-to-solid ratio (LSR), and pH on pectin yield (PY), galacturonic acid (GA) content, and degree of esterification (DE) using a Box-Behnken design. Under optimal conditions (pH 1.2, 7.0â¯min, and 21.5 v/w LSR), we obtained a PY of 28.0⯱â¯0.5%, which was close to the predicted value (31.1%). Second, we analyzed the effect of surfactant on microwave extraction of pectin. Among the surfactants investigated, Tween-80 (8â¯g/L, w/v) increased PY by 17.0%. Compared with conventional solvent extraction, S-MAE is a novel and efficient method for pectin extraction, which generated a higher (pâ¯<â¯0.05) PY (32.8%), GA content (78.1%), DE (69.8%), and Mw (286.3â¯kDa).
Palabras clave
Carbazole (PubChem CID: 6854); D-(+)-galacturonic acid (PubChem CID: 152867); D-(+)-glucose (PubChem CID: 5793); Ethanol (PubChem CID: 702); Extraction; Hydrochloric acid (PubChem CID: 313); Microwave assisted extraction; Optimization; Orange peel pectin; Polyethylene glycol (PubChem CID: 174); Sodium dodecyl sulfate (PubChem CID: 3423265); Sodium hydroxide (PubChem CID: 14798); Surfactant; Tween-20 (PubChem CID: 443314); Tween-80 (PubChem CID: 5281955)
Texto completo:
1
Colección:
01-internacional
Base de datos:
MEDLINE
Asunto principal:
Tensoactivos
/
Pectinas
/
Citrus sinensis
/
Microondas
Idioma:
En
Revista:
Food Chem
Año:
2019
Tipo del documento:
Article
Pais de publicación:
Reino Unido