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N,N-bis-heteroaryl methylamines: Potent anti-mitotic and highly cytotoxic agents.
Khelifi, Ilhem; Naret, Timothée; Hamze, Abdallah; Bignon, Jérome; Levaique, Hélène; Garcia Alvarez, Maria Concepcion; Dubois, Joëlle; Provot, Olivier; Alami, Mouad.
Afiliación
  • Khelifi I; BioCIS, Univ. Paris-Sud, CNRS, Université Paris-Saclay, 92290, Châtenay-Malabry, France.
  • Naret T; BioCIS, Univ. Paris-Sud, CNRS, Université Paris-Saclay, 92290, Châtenay-Malabry, France.
  • Hamze A; BioCIS, Univ. Paris-Sud, CNRS, Université Paris-Saclay, 92290, Châtenay-Malabry, France.
  • Bignon J; CIBI Platform, Institut de Chimie des Substances Naturelles, UPR 2301, CNRS Avenue de la Terrasse, F-91198, Gif sur Yvette, France.
  • Levaique H; CIBI Platform, Institut de Chimie des Substances Naturelles, UPR 2301, CNRS Avenue de la Terrasse, F-91198, Gif sur Yvette, France.
  • Garcia Alvarez MC; CIBI Platform, Institut de Chimie des Substances Naturelles, UPR 2301, CNRS Avenue de la Terrasse, F-91198, Gif sur Yvette, France.
  • Dubois J; CIBI Platform, Institut de Chimie des Substances Naturelles, UPR 2301, CNRS Avenue de la Terrasse, F-91198, Gif sur Yvette, France.
  • Provot O; BioCIS, Univ. Paris-Sud, CNRS, Université Paris-Saclay, 92290, Châtenay-Malabry, France. Electronic address: olivier.provot@u-psud.fr.
  • Alami M; BioCIS, Univ. Paris-Sud, CNRS, Université Paris-Saclay, 92290, Châtenay-Malabry, France. Electronic address: mouad.alami@u-psud.fr.
Eur J Med Chem ; 168: 176-188, 2019 Apr 15.
Article en En | MEDLINE | ID: mdl-30818177
The synthesis and evaluation of a series of N,N-bis-heterocyclic-methylamines 1 as isoazaerianin analogues are described. It was demonstrated that the replacement of the 3,4,5-trimethoxyphenyl A-ring present in CA-4, isoCA-4 and isoazaerianin by a quinoline or a quinazoline ring is possible and often beneficiary for a high level of cytotoxicity. We have also showed that a carbazole or an indole nucleus are very effective as B-rings in this series, leading to anti-cancer drugs 1 having a sub-nanomolar level of cytotoxicity (1a: IC50 = 70 pM against HCT116 cells). 1a also display a high level of cytotoxicity against four other human cancer cells and inhibited tubulin assembly at a micromolar level. Moreover, at a concentration of 5 nM, 1a arrested the cellular cycle in G2/M phase of the cellular cycle and induced apoptosis of HCT116 cells. It was also showed that after few hours 1a at a concentration of 10 nM totally disrupted endothelial network formation on Matrigel.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Citotoxinas / Metilaminas / Mitosis / Antineoplásicos Límite: Humans Idioma: En Revista: Eur J Med Chem Año: 2019 Tipo del documento: Article País de afiliación: Francia Pais de publicación: Francia

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Citotoxinas / Metilaminas / Mitosis / Antineoplásicos Límite: Humans Idioma: En Revista: Eur J Med Chem Año: 2019 Tipo del documento: Article País de afiliación: Francia Pais de publicación: Francia