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Dual-Bioorthogonal Molecular Tool: "Click-to-Release" and "Double-Click" Reactivity on Small Molecules and Material Surfaces.
Luo, Wilson; Luo, Johnny; Popik, Vladimir V; Workentin, Mark S.
Afiliación
  • Luo W; Department of Chemistry and the Centre for Materials and Biomaterials Research , Western University , 1151 Richmond Street , London , Ontario N6A 5B7 , Canada.
  • Luo J; Department of Biochemistry , Western University , London , Ontario N6A 5C1 , Canada.
  • Popik VV; Lawson Health Research Institute , London , Ontario N6C 2R5 , Canada.
  • Workentin MS; Department of Chemistry , University of Georgia , Athens , Georgia 30602 , United States.
Bioconjug Chem ; 30(4): 1140-1149, 2019 04 17.
Article en En | MEDLINE | ID: mdl-30807112
The development of reactive moieties that enable molecular control of bond-forming and bond-breaking reactions within complex media is highly important in materials and biomaterials research as it provides opportunities to carefully manipulate small molecules and material surfaces in a reliable manner. Despite recent advances in the realization of new ligation strategies and "click-and-release" systems, there has been little development of multifunctional moieties that feature a broad range of chemical capabilities. To address this challenge, we designed a molecular tool that can utilize four well-defined bioorthogonal chemistries interchangeably for the attachment, replacement, and release of molecules within a system: the Staudinger-Bertozzi ligation (SBL), perfluoroaryl azide Staudinger reaction (PFAA-SR), strain-promoted alkyne-azide cycloaddition (SPAAC), and strain-promoted alkyne-nitrone cycloaddition (SPANC). We demonstrate "click-to-release" and "double-click" reactivity on small molecules and gold nanoparticles (AuNPs) as a model material substrate. As a proof of concept for material derivatization, we employed 5 nm AuNPs-functionalized with a Rhodamine B derivative and biotin through the double-click strategy-and showed their potential as a pretargeted delivery nanocarrier. This multifunctional molecular tool enables the design and production of molecular and material systems with unique, modular, and tunable dynamic properties that can be altered under mild and bioorthogonal conditions.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Materiales Biocompatibles / Química Clic Idioma: En Revista: Bioconjug Chem Asunto de la revista: BIOQUIMICA Año: 2019 Tipo del documento: Article País de afiliación: Canadá Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Materiales Biocompatibles / Química Clic Idioma: En Revista: Bioconjug Chem Asunto de la revista: BIOQUIMICA Año: 2019 Tipo del documento: Article País de afiliación: Canadá Pais de publicación: Estados Unidos