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Paving the Way for K-Ion Batteries: Role of Electrolyte Reactivity through the Example of Sb-Based Electrodes.
Madec, Lénaïc; Gabaudan, Vincent; Gachot, Grégory; Stievano, Lorenzo; Monconduit, Laure; Martinez, Hervé.
Afiliación
  • Madec L; CNRS/UNIV Pau & Pays Adour/E2S UPPA, Institut des Sciences Analytiques et de Physicochimie pour l'Environnement et les Matériaux, UMR5254 , 64000 Pau , France.
  • Gabaudan V; Réseau sur le Stockage Electrochimique de l'Energie (RS2E), CNRS FR3459 , 33 Rue Saint Leu , 80039 Amiens Cedex, France.
  • Gachot G; ICG-AIME, Bat 15, cc 15-02, Université Montpellier 2 , Pl. E. Bataillon , 34095 Montpellier Cedex 5, France.
  • Stievano L; Réseau sur le Stockage Electrochimique de l'Energie (RS2E), CNRS FR3459 , 33 Rue Saint Leu , 80039 Amiens Cedex, France.
  • Monconduit L; Laboratoire de Réactivité et Chimie des Solide (LRCS) , CNRS, UMR 7314, Université de Picardie Jules Verne , 33 rue Saint Leu , 80039 Amiens , France.
  • Martinez H; Réseau sur le Stockage Electrochimique de l'Energie (RS2E), CNRS FR3459 , 33 Rue Saint Leu , 80039 Amiens Cedex, France.
ACS Appl Mater Interfaces ; 10(40): 34116-34122, 2018 Oct 10.
Article en En | MEDLINE | ID: mdl-30230309
Developing potassium-ion batteries remains a challenge so far due to the lack of efficient electrolytes. Moreover, the high reactivity of K metal and the use of half-cells may greatly alter both the electrochemical performance and the solid electrolyte interphase formation. Here, it is shown that in K metal/Sb half-cells, Coulombic efficiency improvement is achieved by the addition of fluoroethylene carbonate + vinylene carbonate to propylene carbonate (PC), the replacement of PC by ethylene carbonate/diethyl carbonate, and the replacement of KPF6 by potassium bis(fluorosulfonyl)imide. Surprisingly, however, storage of cells containing K metal leads to the coloration of K metal, separators, and Sb electrodes, whereas no change occurs for cells prepared without K metal. These results demonstrate that for all electrolytes, the high electrolyte reactivity with K metal also influences the Sb/electrolyte interface via a cross-talk mechanism. This observation is supported by gas chromatography/mass spectrometry analysis of electrolytes and X-ray photoelectron spectroscopy analysis of Sb electrodes. In summary, these results indicate that the search for efficient electrolytes for potassium-ion batteries must be carried out in full cells if one wants to obtain meaningful correlations between electrochemical performance and electrode/electrolyte interfacial properties. Overall, the results presented here are also likely to benefit the development of other emerging Na- and Mg-ion cell chemistries.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: ACS Appl Mater Interfaces Asunto de la revista: BIOTECNOLOGIA / ENGENHARIA BIOMEDICA Año: 2018 Tipo del documento: Article País de afiliación: Francia Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: ACS Appl Mater Interfaces Asunto de la revista: BIOTECNOLOGIA / ENGENHARIA BIOMEDICA Año: 2018 Tipo del documento: Article País de afiliación: Francia Pais de publicación: Estados Unidos