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Single-Crystal to Single-Crystal Uptake of Volatile Solids and Associated Chromatic Response in a Porous Metallocycle.
du Plessis, Marike; Nikolayenko, Varvara I; Barbour, Leonard J.
Afiliación
  • du Plessis M; Department of Chemistry and Polymer Science , University of Stellenbosch , Matieland 7600 , South Africa.
  • Nikolayenko VI; Department of Chemistry and Polymer Science , University of Stellenbosch , Matieland 7600 , South Africa.
  • Barbour LJ; Department of Chemistry and Polymer Science , University of Stellenbosch , Matieland 7600 , South Africa.
Inorg Chem ; 57(19): 12331-12337, 2018 Oct 01.
Article en En | MEDLINE | ID: mdl-30199233
Guest molecules have been absorbed into crystals of a metallocyclic host by sublimation of volatile solids at room temperature. The guest exchanges are accompanied by color changes. Since the crystals remain intact, evidence of guest inclusion could be obtained using single-crystal X-ray diffraction. The results are also supported by thermogravimetric analysis (TGA), powder X-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FT-IR), and ultraviolet-visible spectroscopy (UV-vis).
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Risk_factors_studies Idioma: En Revista: Inorg Chem Año: 2018 Tipo del documento: Article País de afiliación: Sudáfrica Pais de publicación: Estados Unidos
Texto completo
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XML
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Risk_factors_studies Idioma: En Revista: Inorg Chem Año: 2018 Tipo del documento: Article País de afiliación: Sudáfrica Pais de publicación: Estados Unidos