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Unprecedented Fluorescent Dinuclear CoII and ZnII Coordination Compounds with a Symmetric Bis(salamo)-Like Tetraoxime.
Zhang, Lin-Wei; Liu, Ling-Zhi; Wang, Fei; Dong, Wen-Kui.
Afiliación
  • Zhang LW; School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, 730070, China. zhanglinwei@mail.lzjtu.cn.
  • Liu LZ; School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, 730070, China. llz1009663202@126.com.
  • Wang F; School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, 730070, China. wangfei3986@163.com.
  • Dong WK; School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, 730070, China. dongwk@126.com.
Molecules ; 23(5)2018 May 10.
Article en En | MEDLINE | ID: mdl-29748523
Two unprecedented homometallic CoII and ZnII coordination compounds, [M2(L)(OCH3)][M2(L)(OAc)] (MII = CoII (1) and ZnII (2)), with a novel symmetric bis(salamo)-like tetraoxime ligand H3L were synthesized and characterized by elemental analyses, infrafred (IR), ultraviolet⁻visible spectroscopy (UV-Vis), fluorescent spectra and single-crystal X-ray diffraction analyses. The unit cell of the two coordination compounds contains two crystallographically and chemically independent dinuclear coordination compounds. In the two coordination compounds, three metal ions are five-coordinated, formed two square pyramidal and a trigonal bipyramidal geometries, and the other metal ion is a hexacoordinate octahedral configuration. In addition, the coordination compound 1 forms a 3D supramolecular structure, and the coordination compound 2 forms a 0D dimer structure by the inter-molecular hydrogen bond interactions. Meanwhile, the fluorescence spectra of the coordination compounds 1 and 2 were also measured and discussed.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Oximas / Zinc / Cobalto / Complejos de Coordinación Idioma: En Revista: Molecules Asunto de la revista: BIOLOGIA Año: 2018 Tipo del documento: Article País de afiliación: China Pais de publicación: Suiza

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Oximas / Zinc / Cobalto / Complejos de Coordinación Idioma: En Revista: Molecules Asunto de la revista: BIOLOGIA Año: 2018 Tipo del documento: Article País de afiliación: China Pais de publicación: Suiza