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Long-lasting ergot lipids as new biomarkers for assessing the presence of cereals and cereal products in archaeological vessels.
Lucejko, Jeannette J; La Nasa, Jacopo; Porta, Francesca; Vanzetti, Alessandro; Tanda, Giuseppa; Mangiaracina, Claudio Filippo; Corretti, Alessandro; Colombini, Maria Perla; Ribechini, Erika.
Afiliación
  • Lucejko JJ; Dipartimento di Chimica e Chimica Industriale, Università di Pisa, Via G. Moruzzi 13, 56124, Pisa, Italy.
  • La Nasa J; Dipartimento di Chimica e Chimica Industriale, Università di Pisa, Via G. Moruzzi 13, 56124, Pisa, Italy.
  • Porta F; Dipartimento di Scienze dell'Antichità, Università degli Studi di Roma "La Sapienza", Piazzale Aldo Moro, 5, 00185, Roma, Italy.
  • Vanzetti A; Dipartimento di Scienze dell'Antichità, Università degli Studi di Roma "La Sapienza", Piazzale Aldo Moro, 5, 00185, Roma, Italy.
  • Tanda G; Dipartimento di Storia, Beni Culturali e Territorio, Università degli Studi di Cagliari, Piazza Arsenale 1, 09124, Cagliari, Italy.
  • Mangiaracina CF; LA3M, Aix Marseille Université, CNRS, rue du château de l'Horloge 5, 13094, Aix-en-Provence, France.
  • Corretti A; Laboratorio di Storia, Archeologia, Epigrafia, Tradizione dell'antico, Scuola Normale Superione, Piazza dei Cavalieri, 56126, Pisa, Italy.
  • Colombini MP; Dipartimento di Chimica e Chimica Industriale, Università di Pisa, Via G. Moruzzi 13, 56124, Pisa, Italy.
  • Ribechini E; Dipartimento di Chimica e Chimica Industriale, Università di Pisa, Via G. Moruzzi 13, 56124, Pisa, Italy. erika.ribechini@unipi.it.
Sci Rep ; 8(1): 3935, 2018 03 02.
Article en En | MEDLINE | ID: mdl-29500428
Cereals were very important in ancient diets, however evidence from archaeological sites of the vessels used for processing or storing cereals is comparatively rare. Micro-organisms, as well as chemical-physical effects can easily degrade cereals during the burial period. This can lead to a complete cereal decay and to serious difficulties in estimating the intensity of use of the cereals by ancient populations. Here, we present a novel biomarker approach entailing the detection of secondary lipid metabolites produced by ergot fungi (genus Claviceps), which are common cereal pests. The aim was to identify the original presence of Gramineae and to indirectly establish if vessels were used for cereal storage/processing. The fatty acid and TAG-estolide profiles of the remains from more than 30 archaeological vessels were investigated by gas chromatography/mass spectrometry (GC/MS) and high performance liquid chromatography/high resolution mass spectrometry (HPLC/ESI-Q-ToF). The detection of lipids derived from ergot in archaeological and historic contexts rests on its complex chemistry, providing a unique and relatively recalcitrant chemical signature for cereals. This research demonstrated that the combination of our innovative biomarker approach along with environmental and archaeological evidence can provide unprecedented insights into the incidence of cereals and related processing activities in ancient societies.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Arqueología / Grano Comestible / Claviceps / Lípidos Tipo de estudio: Prognostic_studies País/Región como asunto: Europa Idioma: En Revista: Sci Rep Año: 2018 Tipo del documento: Article País de afiliación: Italia Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Arqueología / Grano Comestible / Claviceps / Lípidos Tipo de estudio: Prognostic_studies País/Región como asunto: Europa Idioma: En Revista: Sci Rep Año: 2018 Tipo del documento: Article País de afiliación: Italia Pais de publicación: Reino Unido