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Evidence of a cubic iron sub-lattice in t-CuFe2O4 demonstrated by X-ray Absorption Fine Structure.
Caddeo, Francesco; Loche, Danilo; Casula, Maria F; Corrias, Anna.
Afiliación
  • Caddeo F; School of Physical Sciences, Ingram Building, University of Kent, Canterbury, CT2 7NH, United Kingdom.
  • Loche D; ZIK SiLi-nano, Martin-Luther-University Halle-Wittenberg, Karl-Freiherr-von-Fritsch-Straße 3, 06120, Halle (Saale), Germany.
  • Casula MF; School of Physical Sciences, Ingram Building, University of Kent, Canterbury, CT2 7NH, United Kingdom.
  • Corrias A; INSTM and Dipartimento di Scienze Chimiche e Geologiche, Università di Cagliari, S.S. 554, bivio per Sestu, Monserrato, CA, Italy.
Sci Rep ; 8(1): 797, 2018 01 15.
Article en En | MEDLINE | ID: mdl-29335500
Copper ferrite, belonging to the wide and technologically relevant class of spinel ferrites, was grown in the form of t-CuFe2O4 nanocrystals within a porous matrix of silica in the form of either an aerogel or a xerogel, and compared to a bulk sample. Extended X-ray absorption fine structure (EXAFS) spectroscopy revealed the presence of two different sub-lattices within the crystal structure of t-CuFe2O4, one tetragonal and one cubic, defined by the Cu2+ and Fe3+ ions respectively. Our investigation provides evidence that the Jahn-Teller distortion, which occurs on the Cu2+ ions located in octahedral sites, does not affect the coordination geometry of the Fe3+ ions, regardless of their location in octahedral or tetrahedral sites.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Sci Rep Año: 2018 Tipo del documento: Article País de afiliación: Reino Unido Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Sci Rep Año: 2018 Tipo del documento: Article País de afiliación: Reino Unido Pais de publicación: Reino Unido