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Substituted Benzamides from Anti-inflammatory and p38 Kinase Inhibitors to Antitubercular Activity: Design, Synthesis and Screening.
Kulkarni, Ravindra; Mitkari, Umakant; Achaiah, G; Laufer, Stefan; Bikshapti, D V R N; Chandrashekar, V M; Gurav, P B; Joshi, S J; Chipade, V D.
Afiliación
  • Kulkarni R; SVERI's College of Pharmacy, Gopalpur Road, Pandharpur-413 304, Maharashtra State, India.
  • Mitkari U; University College of Pharmaceutical Sciences, Kakatiya University, Warangal, Andhra Pradesh, India.
  • Achaiah G; SVERI's College of Pharmacy, Gopalpur Road, Pandharpur-413 304, Maharashtra State, India.
  • Laufer S; University College of Pharmaceutical Sciences, Kakatiya University, Warangal, Andhra Pradesh, India.
  • Bikshapti DVRN; Institute of Pharmacy, Department of Pharmaceutical and Medicinal Chemistry, Eberhard-Karls-University, Tubingen, Auf der Morgenstelle, 8, 72076, Germany.
  • Chandrashekar VM; Vijaya College of Pharmacy, Hayatnagar, Hyderabad, India.
  • Gurav PB; BVVS's Hanagal Shri Kumareshwar College of Pharmacy, BVVS Campus, Bagalkot, Karnataka 587 101, India.
  • Joshi SJ; SVERI's College of Pharmacy, Gopalpur Road, Pandharpur-413 304, Maharashtra State, India.
  • Chipade VD; SVERI's College of Pharmacy, Gopalpur Road, Pandharpur-413 304, Maharashtra State, India.
Mini Rev Med Chem ; 18(17): 1486-1497, 2018.
Article en En | MEDLINE | ID: mdl-28685700
BACKGROUND: Twenty one amide compounds possessing phenoxy/benzyloxy/pyridinyl groups have been synthesized by benzoylation of respective amines in presence of base with moderate to encouraging yields. Upon confirmation of structure, compounds were subjected for p38 kinase inhibitory, anti-inflammatory, antimicrobial and antitubercular activities. METHOD: Anti-inflammatory activity was determined using carrageenan induced rat paw edema model while p38 kinase inhibitory activity was studied using ELISA method and serial dilution method was employed to determine MICs. Two compounds 4g and 4n showed over 30% p38 kinase inhibitory activity at 10 µM and best anti-inflammatory activity was found for compounds 4g, 4i, 4n and 4o which exhibited to reduce paw edema over 70%. Compound 4b was observed to be the most potent against gram +ve organisms with MIC value of 1.6 µG/mL and compound 4u displayed potent antibacterial activity against gram negative organisms. CONCLUSION: Most encouraging antitubercular activity was noticed for compounds 4u, 4r and 4k with 6.25, 12.5 and 12.5 µG/mL Further, in order to know the binding site interactions, a docking simulations of compounds was performed. These preliminary results will certainly show fruitful directions to improve the activities of compounds.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Benzamidas / Antiinflamatorios no Esteroideos / Proteínas Quinasas p38 Activadas por Mitógenos / Inhibidores de Proteínas Quinasas / Edema / Antibacterianos / Antifúngicos Tipo de estudio: Diagnostic_studies / Screening_studies Límite: Animals / Humans Idioma: En Revista: Mini Rev Med Chem Asunto de la revista: QUIMICA Año: 2018 Tipo del documento: Article País de afiliación: India Pais de publicación: Países Bajos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Benzamidas / Antiinflamatorios no Esteroideos / Proteínas Quinasas p38 Activadas por Mitógenos / Inhibidores de Proteínas Quinasas / Edema / Antibacterianos / Antifúngicos Tipo de estudio: Diagnostic_studies / Screening_studies Límite: Animals / Humans Idioma: En Revista: Mini Rev Med Chem Asunto de la revista: QUIMICA Año: 2018 Tipo del documento: Article País de afiliación: India Pais de publicación: Países Bajos