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Resolving Electronic Transitions in Synthetic Fluorescent Protein Chromophores by Magnetic Circular Dichroism.
Stepánek, Petr; Cowie, Thomas Y; Safarík, Martin; Sebestík, Jaroslav; Pohl, Radek; Bour, Petr.
Afiliación
  • Stepánek P; NMR Research Group, Faculty of Science, University of Oulu, PO Box 3000, 90014, Oulu, Finland.
  • Cowie TY; Institute of Organic Chemistry and Biochemistry, AS CR, Flemingovo námestí 2, 166 10, Prague, Czech Republic.
  • Safarík M; Institute of Organic Chemistry and Biochemistry, AS CR, Flemingovo námestí 2, 166 10, Prague, Czech Republic.
  • Sebestík J; Institute of Organic Chemistry and Biochemistry, AS CR, Flemingovo námestí 2, 166 10, Prague, Czech Republic.
  • Pohl R; Institute of Organic Chemistry and Biochemistry, AS CR, Flemingovo námestí 2, 166 10, Prague, Czech Republic.
  • Bour P; Institute of Organic Chemistry and Biochemistry, AS CR, Flemingovo námestí 2, 166 10, Prague, Czech Republic. bour@uochb.cas.cz.
Chemphyschem ; 17(15): 2348-54, 2016 Aug 04.
Article en En | MEDLINE | ID: mdl-27124359
The detailed electronic structures of fluorescent chromophores are important for their use in imaging of living cells. A series of green fluorescent protein chromophore derivatives is examined by magnetic circular dichroism (MCD) spectroscopy, which allows the resolution of more bands than plain absorption and fluorescence. Observed spectral patterns are rationalized with the aid of time-dependent density functional theory (TDDFT) computations and the sum-over-state (SOS) formalism, which also reveals a significant dependence of MCD intensities on chromophore conformation. The combination of organic and theoretical chemistry with spectroscopic techniques also appears useful in the rational design of fluorescence labels and understanding of the chromophore's properties. For example, the absorption threshold can be heavily affected by substitution on the phenyl ring but not much on the five-member ring, and methoxy groups can be used to further tune the electronic levels.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Dicroismo Circular / Electrones / Colorantes Fluorescentes / Proteínas Luminiscentes Idioma: En Revista: Chemphyschem Asunto de la revista: BIOFISICA / QUIMICA Año: 2016 Tipo del documento: Article País de afiliación: Finlandia Pais de publicación: Alemania

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Dicroismo Circular / Electrones / Colorantes Fluorescentes / Proteínas Luminiscentes Idioma: En Revista: Chemphyschem Asunto de la revista: BIOFISICA / QUIMICA Año: 2016 Tipo del documento: Article País de afiliación: Finlandia Pais de publicación: Alemania