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A rapid HPLC method for plasma and serum mexiletine determination and its use in therapeutic drug monitoring.
Paczkowski, D; Podlesny, J; Filipek, M.
Afiliación
  • Paczkowski D; Department of Diagnostics Laboratory, Memorial Hospital-Child Health Centre, Warszawa, Poland.
Pol J Pharmacol Pharm ; 41(5): 459-67, 1989.
Article en En | MEDLINE | ID: mdl-2641399
A HPLC method for the determination of mexiletine in human plasma and serum is described. Serum or plasma after addition of mexiletine and internal standard was extracted with diisopropyl ether. The extract was then evaporated and dissolved in the mobile phase. An aliquot of the solution was chromatographed on a reversed-phase C8 column. The peaks were detected by UV (214 nm) at room temperature. The limit of detection of mexiletine was approximately 0.02 mg/l of plasma or serum. The validity of the method is discussed and compared with other methods.
Asunto(s)
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Mexiletine Límite: Humans Idioma: En Revista: Pol J Pharmacol Pharm Año: 1989 Tipo del documento: Article País de afiliación: Polonia Pais de publicación: Polonia
Buscar en Google
Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Mexiletine Límite: Humans Idioma: En Revista: Pol J Pharmacol Pharm Año: 1989 Tipo del documento: Article País de afiliación: Polonia Pais de publicación: Polonia