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Simultaneous Interaction of Hydrophilic and Hydrophobic Solvents with Ethylamino Neurotransmitter Radical Cations: Infrared Spectra of Tryptamine(+)-(H2O)m-(N2)n Clusters (m,n ≤ 3).
Schütz, Markus; Sakota, Kenji; Moritz, Raphael; Schmies, Matthias; Ikeda, Takamasa; Sekiya, Hiroshi; Dopfer, Otto.
Afiliación
  • Schütz M; Institut für Optik und Atomare Physik, Technische Universität Berlin , D-10623 Berlin, Germany.
  • Sakota K; Department of Chemistry, Faculty of Sciences, and Department of Molecular Chemistry, Graduate School of Science, Kyushu University , 6-10-1 Hakozaki, Higashi-ku, Fukuoka 812-8581, Japan.
  • Moritz R; Institut für Optik und Atomare Physik, Technische Universität Berlin , D-10623 Berlin, Germany.
  • Schmies M; Institut für Optik und Atomare Physik, Technische Universität Berlin , D-10623 Berlin, Germany.
  • Ikeda T; Department of Chemistry, Faculty of Sciences, and Department of Molecular Chemistry, Graduate School of Science, Kyushu University , 6-10-1 Hakozaki, Higashi-ku, Fukuoka 812-8581, Japan.
  • Sekiya H; Department of Chemistry, Faculty of Sciences, and Department of Molecular Chemistry, Graduate School of Science, Kyushu University , 6-10-1 Hakozaki, Higashi-ku, Fukuoka 812-8581, Japan.
  • Dopfer O; Institut für Optik und Atomare Physik, Technische Universität Berlin , D-10623 Berlin, Germany.
J Phys Chem A ; 119(39): 10035-51, 2015 Oct 01.
Article en En | MEDLINE | ID: mdl-26353045
Solvation of biomolecules by a hydrophilic and hydrophobic environment strongly affects their structure and function. Here, the structural, vibrational, and energetic properties of size-selected clusters of the microhydrated tryptamine cation with N2 ligands, TRA(+)-(H2O)m-(N2)n (m,n ≤ 3), are characterized by infrared photodissociation spectroscopy in the 2800-3800 cm(-1) range and dispersion-corrected density functional theory calculations at the ωB97X-D/cc-pVTZ level to investigate the simultaneous solvation of this prototypical neurotransmitter by dipolar water and quadrupolar N2 ligands. In the global minimum structure of TRA(+)-H2O generated by electron ionization, H2O is strongly hydrogen-bonded (H-bonded) as proton acceptor to the acidic indolic NH group. In the TRA(+)-H2O-(N2)n clusters, the weakly bonded N2 ligands do not affect the H-bonding motif of TRA(+)-H2O and are preferentially H-bonded to the OH groups of the H2O ligand, whereas stacking to the aromatic π electron system of the pyrrole ring of TRA(+) is less favorable. The natural bond orbital analysis reveals that the H-bond between the N2 ligand and the OH group of H2O cooperatively strengthens the adjacent H-bond between the indolic NH group of TRA(+) and H2O, while π stacking is slightly noncooperative. In the larger TRA(+)-(H2O)m clusters, the H2O ligands form a H-bonded solvent network attached to the indolic NH proton, again stabilized by strong cooperative effects arising from the nearby positive charge. Comparison with the corresponding neutral TRA-(H2O)m clusters illustrates the strong impact of the excess positive charge on the structure of the microhydration network.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Solventes / Agua / Triptaminas / Neurotransmisores / Etilaminas / Nitrógeno Idioma: En Revista: J Phys Chem A Asunto de la revista: QUIMICA Año: 2015 Tipo del documento: Article País de afiliación: Alemania Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Solventes / Agua / Triptaminas / Neurotransmisores / Etilaminas / Nitrógeno Idioma: En Revista: J Phys Chem A Asunto de la revista: QUIMICA Año: 2015 Tipo del documento: Article País de afiliación: Alemania Pais de publicación: Estados Unidos