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Single and multi-component adsorption of salicylic acid, clofibric acid, carbamazepine and caffeine from water onto transition metal modified and partially calcined inorganic-organic pillared clay fixed beds.
Cabrera-Lafaurie, Wilman A; Román, Félix R; Hernández-Maldonado, Arturo J.
Afiliación
  • Cabrera-Lafaurie WA; Department of Chemical Engineering, University of Puerto Rico-Mayagüez Campus, Mayagüez, PR 00681-9000 United States.
  • Román FR; Department of Chemistry, University of Puerto Rico-Mayagüez Campus, Mayagüez, PR 00681-9000 United States.
  • Hernández-Maldonado AJ; Department of Chemical Engineering, University of Puerto Rico-Mayagüez Campus, Mayagüez, PR 00681-9000 United States. Electronic address: arturoj.hernandez@upr.edu.
J Hazard Mater ; 282: 174-82, 2015 Jan 23.
Article en En | MEDLINE | ID: mdl-24680542
Fixed-beds of transition metal (Co(2+), Ni(2+) or Cu(2+)) inorganic-organic pillared clays (IOCs) were prepared to study single- and multi-component non-equilibrium adsorption of a set of pharmaceutical and personal care products (PPCPs: salicylic acid, clofibric acid, carbamazepine and caffeine) from water. Adsorption capacities for single components revealed that the copper(II) IOCs have better affinity toward salicylic and clofibric acid. However, multi-component adsorption tests showed a considerable decrease in adsorption capacity for the acids and an unusual selectivity toward carbamazepine depending on the transition metal. This was attributed to a combination of competition between PPCPs for adsorption sites, adsorbate-adsorbate interactions, and plausible pore blocking caused by carbamazepine. The cobalt(II) IOC bed that was partially calcined to fractionate the surfactant moiety showcased the best selectivity toward caffeine, even during multi-component adsorption. This was due to a combination of a mildly hydrophobic surface and interaction between the PPCP and cobalt(II). In general, the tests suggest that these IOCs may be a potential solution for the removal of PPCPs if employed in a layered-bed configuration, to take care of families of adsorbates in a sequence that would produce sharpened concentration wavefronts.
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Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Contaminantes Químicos del Agua / Bentonita / Preparaciones Farmacéuticas / Cobalto / Cobre / Níquel Idioma: En Revista: J Hazard Mater Asunto de la revista: SAUDE AMBIENTAL Año: 2015 Tipo del documento: Article Pais de publicación: Países Bajos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Contaminantes Químicos del Agua / Bentonita / Preparaciones Farmacéuticas / Cobalto / Cobre / Níquel Idioma: En Revista: J Hazard Mater Asunto de la revista: SAUDE AMBIENTAL Año: 2015 Tipo del documento: Article Pais de publicación: Países Bajos