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Intense chiroptical switching in a dicationic helicene-like derivative: exploration of a viologen-type redox manifold of a non-racemic helquat.
Pospísil, Lubomír; Bednárová, Lucie; Stepánek, Petr; Slavícek, Petr; Vávra, Jan; Hromadová, Magdaléna; Dlouhá, Helena; Tarábek, Ján; Teplý, Filip.
Afiliación
  • Pospísil L; Institute of Organic Chemistry and Biochemistry, Academy of Sciences of the Czech Republic , 16610 Prague, Czech Republic.
J Am Chem Soc ; 136(31): 10826-9, 2014 Aug 06.
Article en En | MEDLINE | ID: mdl-24597856
Two-step redox switching in enantiopure helquat system [P-1](2+) ⇌ [P-1](•+) ⇌ [P-1](0) is demonstrated. The viologen-type electroactive unit embedded directly in the helical scaffold of 1 is responsible for the prominent chiroptical switching at 264 nm. This process is associated with a marked sign-reversal of Cotton effect ramping between Δε = +35 M(-1) cm(-1) for [P-1](2+) and Δε = -100 M(-1) cm(-1) for [P-1](0). This helically chiral system features the most intense chiroptical switch response documented in the field of helicenoids.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: J Am Chem Soc Año: 2014 Tipo del documento: Article País de afiliación: República Checa Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: J Am Chem Soc Año: 2014 Tipo del documento: Article País de afiliación: República Checa Pais de publicación: Estados Unidos