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Residue Val237 is critical for the enantioselectivity of Penicillium expansum lipase.
Tang, Lianghua; Su, Min; Chi, Liying; Zhang, Junling; Zhang, Huihui; Zhu, Ling.
Afiliación
  • Tang L; College of Life Sciences, Fujian Normal University, Fuzhou, 350108, China, biotlh@gmail.com.
Biotechnol Lett ; 36(3): 633-9, 2014 Mar.
Article en En | MEDLINE | ID: mdl-24338160
The shape of the hydrophobic tunnel leading to the active site of Penicillium expansum lipase (PEL) was redesigned by single-point mutations, in order to better understand enzyme enantioselectivity towards naproxen. A variant with a valine-to-glycine substitution at residue 237 exhibited almost no enantioselectivity (E = 1.1) compared with that (E = 104) of wild-type PEL. The function of the residue, Val237, in the hydrophobic tunnel was further analyzed by site-directed mutagenesis. For each of these variants a significant decrease of enantioselectivity (E < 7) was observed compared with that of wild-type enzyme. Further docking result showed that Val237 plays the most important role in stabilizing the correct orientation of (R)-naproxen. Overall, these results indicate that the residue Val237 is the key amino acid residue maintaining the enantioselectivity of the lipase.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Penicillium / Valina / Naproxeno / Lipasa Idioma: En Revista: Biotechnol Lett Año: 2014 Tipo del documento: Article Pais de publicación: Países Bajos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Penicillium / Valina / Naproxeno / Lipasa Idioma: En Revista: Biotechnol Lett Año: 2014 Tipo del documento: Article Pais de publicación: Países Bajos