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Mechanism of inhibition of Mycobacterium tuberculosis antigen 85 by ebselen.
Favrot, Lorenza; Grzegorzewicz, Anna E; Lajiness, Daniel H; Marvin, Rachel K; Boucau, Julie; Isailovic, Dragan; Jackson, Mary; Ronning, Donald R.
Afiliación
  • Favrot L; Department of Chemistry, University of Toledo, Toledo, Ohio 43606-3390, USA.
Nat Commun ; 4: 2748, 2013.
Article en En | MEDLINE | ID: mdl-24193546
The increasing prevalence of drug-resistant tuberculosis highlights the need for identifying new antitubercular drugs that can treat these infections. The antigen 85 (Ag85) complex has emerged as an intriguing mycobacterial drug target due to its central role in synthesizing major components of the inner and outer leaflets of the mycobacterial outer membrane. Here we identify ebselen (EBS) as a potent inhibitor of the Mycobacterium tuberculosis Ag85 complex. Mass spectrometry data show that EBS binds covalently to a cysteine residue (C209) located near the Ag85C active site. The crystal structure of Ag85C in the presence of EBS shows that C209 modification restructures the active site, thereby disrupting the hydrogen-bonded network within the active site that is essential for enzymatic activity. C209 mutations display marked decreases in enzymatic activity. These data suggest that compounds using this mechanism of action will strongly inhibit the Ag85 complex and minimize the selection of drug resistance.
Asunto(s)

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Azoles / Regulación Bacteriana de la Expresión Génica / Antiinflamatorios no Esteroideos / Compuestos de Organoselenio / Mycobacterium tuberculosis / Antígenos Bacterianos Tipo de estudio: Risk_factors_studies Idioma: En Revista: Nat Commun Asunto de la revista: BIOLOGIA / CIENCIA Año: 2013 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Reino Unido

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Azoles / Regulación Bacteriana de la Expresión Génica / Antiinflamatorios no Esteroideos / Compuestos de Organoselenio / Mycobacterium tuberculosis / Antígenos Bacterianos Tipo de estudio: Risk_factors_studies Idioma: En Revista: Nat Commun Asunto de la revista: BIOLOGIA / CIENCIA Año: 2013 Tipo del documento: Article País de afiliación: Estados Unidos Pais de publicación: Reino Unido