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Simple and sensitive synchronous- fluorescence method for the determination of trace bisphenol S based on its inhibitory effect on the fluorescence quenching reaction of rhodamine B.
Cao, Gui-ping; Chen, Ting; Zhuang, Ya-feng.
Afiliación
  • Cao GP; Department of Chemical Engineering, Changzhou Institute of Technology, Changzhou, Jiangsu, 213022, People's Republic of China, caogpczu@163.com.
J Fluoresc ; 23(4): 641-7, 2013 Jul.
Article en En | MEDLINE | ID: mdl-23471627
An inhibitory kinetic fluorimetric method is reported for the determination of trace bisphenol S (BPS). The proposed method is based on the inhibitory effect of BPS on the fluorescence quenching of rhodamine B (RhB) caused by potassium bromate in a dilute phosphoric acid medium. Under the optimal conditions of the experiment, the detection limit for BPS was 0.021 mg/L, and the linear range of determination was from 0.035 mg/L to 0.750 mg/L. The relative standard deviations of 11 measurements for 0.20 mg/L and 0.40 mg/L BPS solutions were 2.74 % and 1.87 %, respectively. The method was successfully applied to the determination of bisphenol S derived from commercially available plastic film samples in hot water. A possible reaction mechanism of the inhibitory effect of BPS on the fluorescence quenching of RhB was proposed.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: J Fluoresc Asunto de la revista: BIOFISICA Año: 2013 Tipo del documento: Article Pais de publicación: Países Bajos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Tipo de estudio: Diagnostic_studies Idioma: En Revista: J Fluoresc Asunto de la revista: BIOFISICA Año: 2013 Tipo del documento: Article Pais de publicación: Países Bajos