Enhanced NMR-based profiling of polyphenols in commercially available grape juices using solid-phase extraction.
Magn Reson Chem
; 49 Suppl 1: S27-36, 2011 Dec.
Article
en En
| MEDLINE
| ID: mdl-22290706
Grapes and related products, such as juices, and in particular, their polyphenols, have previously been associated with many health benefits, such as protection against cardiovascular disease. Within grapes, a large range of structurally diverse polyphenols can be present, and their characterisation stands as a challenge. (1)H NMR spectroscopy in principle would provide a rapid, nondestructive and straightforward method for profiling of polyphenols. However, polyphenol profiling and identification in grape juices is hindered because of signals of prevailing carbohydrates causing spectral overlap and compromising dynamic range. This study describes the development of an extraction method prior to analysis using (1)H NMR spectroscopy, which can, potentially, significantly increase the number of detectable polyphenols and aid their identification, by reduction of signal overlap and selective removal of heavily dominating compounds such as sugars.
Texto completo:
1
Colección:
01-internacional
Base de datos:
MEDLINE
Asunto principal:
Vitis
/
Extracción en Fase Sólida
/
Polifenoles
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Tecnología de Alimentos
Idioma:
En
Revista:
Magn Reson Chem
Asunto de la revista:
QUIMICA
Año:
2011
Tipo del documento:
Article
Pais de publicación:
Reino Unido