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New Dendrimers: Synthesis and Characterization of Popam - Pamam Hybrid Dendrimers.
Majoros, István J; Williams, Christopher R; Tomalia, Donald A; Baker, James R.
Afiliación
  • Majoros IJ; Department of Internal Medicine, Division of Allergy, Michigan Nanotechnology Institute for Medicine and Biological Sciences, Macromolecular Science and Engineering, University of Michigan, Ann Arbor, MI 48109-0533, www.nano.med.umich.edu.
Macromolecules ; 41(22): 8372-8379, 2008 Nov 25.
Article en En | MEDLINE | ID: mdl-21258604
Recently developed multifunctional cancer therapeutic nano-device production is based on poly(amidoamine) PAMAM generation 5 (G5) dendrimer as a carrier 1-5. Scale up synthesis of this nano-device is limited because of long reaction sequence (12 reaction steps) and long and not easy work up of the products after each reaction step. Combination of poly(propyle-imine) and poly(amidoamine) synthesis can improve the production of the drug carrier.In this paper we give a general overview of the synthesis and characterization of a series of novel hybrid dendrimers which we coined as novel POMAM hybrid dendrimers, constructed from poly(propylene-imine) (PPI or POPAM) core and poly(amidoamine) PAMAM shells. The synthesis was accomplished by a divergent reiterating method involving repeating subsequent Michael addition and amidation reactions. Each generation of the newly synthesized dendrimer was characterized by using HPLC, GPC, NMR and AFM.

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Macromolecules Año: 2008 Tipo del documento: Article Pais de publicación: Estados Unidos

Texto completo: 1 Colección: 01-internacional Base de datos: MEDLINE Idioma: En Revista: Macromolecules Año: 2008 Tipo del documento: Article Pais de publicación: Estados Unidos