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The development of a radioimmunoassay system for testosterone (T) and dihydrotestosterone (DHT). Part 1. The preparation of the T-derivatives and T-protein conjugates.
Neacsu, E; Oniciu, D; Simionescu, L.
Afiliación
  • Neacsu E; C. I. Parhon Institute of Endocrinology, Bucharest, Romania.
Endocrinologie ; 28(1): 25-31, 1990.
Article en En | MEDLINE | ID: mdl-2080417
Testosterone-17-hemisuceinate (T-17-HS) by esterification with succinic anhydride technique and Testosterone-3-carboxy-methyl-oxyme (T-3-CMO) derivatives were synthesized. The T-protein (BSA) conjugates were prepared by the condensation with carbodiimide technique, for the T-17-HS derivative and by the mixed anhydride technique, for the T-3-CMO. Both the derivatives and the T-BSA conjugates were characterized by melting point, ultraviolet and infrared spectra, thin layer chromatography. The physico-chemical characteristics and the hapten-protein incorporation being convenient: 28 mol T/mol BSA for T-17-HS-BSA and 38 mol T/mol BSA for T-3-CMO-BSA, the T-carrier conjugates are adequate for their use as immunogens.
Asunto(s)
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Dihidrotestosterona / Testosterona / Radioinmunoensayo Límite: Animals / Humans Idioma: En Revista: Endocrinologie Año: 1990 Tipo del documento: Article País de afiliación: Rumanía Pais de publicación: Rumanía
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Colección: 01-internacional Base de datos: MEDLINE Asunto principal: Dihidrotestosterona / Testosterona / Radioinmunoensayo Límite: Animals / Humans Idioma: En Revista: Endocrinologie Año: 1990 Tipo del documento: Article País de afiliación: Rumanía Pais de publicación: Rumanía